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Pesticide CCV chromatogram data, sample AD27193, Dec 2001

Machine-extracted title · confidence 95%

Chromatogram and signal data for chlorinated pesticide quality control verification in sample AD27193.

NYC-WTC_000090244–000090249

Folder label: “508 X 11/14/01 A 12/12/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Signal #1 : C:\HPCHEM\l\DATA\508F\011212\2PESTC2.D\ECDlA.CH Vial: 56 Signal #2 : C:\HPCHEM\l\DATA\508F\011212\2PESTC2.D\ECD2B.CH Acq On : 13 Dec 2001 10:07 am Operator: Nefliu Sample : pest ccv2 Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Dec 13 12:05 2001 Quant Results File: 011205P.RES Quant Method : C:\HPCHEM\1\METHODS\508\011205P.M (Chemstation Integrator)' Title : 508 CHLORINATED PESTICIDES 9/6/00 Last Update : Sun Oct 21 15:26:52 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M Volume Inj . Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/L ug/L

System Monitoring Compounds LO) S 2,4-DDD SURROGAT 36.33f 33.62 996844 1181671 0.171 0.199m Spilced Amount 0.2 00 Recovery = 85.50% 99.50% Target Compounds 1) PROPACHLOR 16.05f 15.20 165823 167607 0.167m/'tt 0.166 2) g-BHC 22.08f 20.08 2784379 3563130 0.271 'll/ 0.270 3) HEPTACHLOR 24.70f 21.45 590610 799090 0.080m/i/. 0.077m 4) ALDRIN 27.40f 23.49 1349539 1510053 0.115m<?U 0.115 5) HEPTACHLOR EPOXI 31.46f 28.78 2313200 2704948 0.231mgZ> 0.232 6) 4,4'-DDE 34.99f 31.96 3937118 4512326 0.402m,p(/ 0.396 7) DIELDRIN 35.24f 32.61 667047 878710 0.070mJ/.} 0.076 8) ENDRIN 37.19f 33.66 1227808 1635820 0.228m (|b-( 0.187m 9) METHOXYCHLOR 47.77f 40.55 826141 959878 0.330m 0.295

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 011205P.M Eri Dec 21 13:42:40 2001 Page 1

NYC-WTC_000090244

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NYC-WTC_000090244Source: NYC Law Department, mirrored locally

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