NYC Law Department release
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← Document results/DEP Box 68/508 X 11/13/01 A 12/7/01
Document / 2 pages

PCB Arochlor 1260 analysis data, Dec 2001

Machine-extracted title · confidence 95%

Quality control log documenting PCB Arochlor 1260 spike recovery percentages and analytical responses from December 2001 testing.

NYC-WTC_000090018–000090019

Folder label: “508 X 11/13/01 A 12/7/01

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Scanned page image, NYC-WTC_000090018
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\MSDCHEM\l\DATA\508\011207\PRL1260.D\ECDlA.CH Vial: 67 Signal #2 : C:\MSDCHEM\1\DATA\5O8\O112O7\PRL126O.D\ECD2B.CH Acq On : 08 Dec 2001 9:47 pm Operator: Nefliu Sample : prl 1260 Inst : Instrume Mise : Multiplr: 1.00 IntFile Signal #1: EVENTS.E IntFile Signal #2: events2.e Quant Time: Dec 20 16:35:39 2001 Quant Results File: PCB1260.RES

Quant Method : C:\MSDCHEM\1\METHODS\PCB1260.M (Chemstation Integrator) Title : 508 - Arochlor 1260 Last Update : Tue Dec 18 09:56:02 2001 Response via : Initial Calibration > DataAcq Meth : MDL508.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 Conc#l Conc#2

System Monitoring Compounds 6) s 2,4-DDD SURROGAT 14.46 15.05 548.3E6 430.8E6/ 6.193 A 0.171 Spiked Amount 0.200 Recovery = / 96.50% y 85.50% Target Compounds 2) 1260 - peak 2 13.42 0.00 2015381 0 0.014 N.D. d# 3) 1260 - peak 3 14.71 15.77 2995866 1436018 0.009m 0.005m# 4) 1260 - peak 4 15.32 0.00 4601417 0 0.011 N.D. d# 5) 1260 - peak 5 17.38 17.91 4779074 2194557 0.010 0.005m#

9

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. PRL1260.'D PCB1260.M Thu Dec 20 16:36:44 2001 Page 1

NYC-WTC_000090018

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NYC-WTC_000090018Source: NYC Law Department, mirrored locally

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