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GC/MS analysis results for sample AD23833, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089461–000089475

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Quantitation Report '(QT- Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 31 12:27 2001 Quant Results File: NP10190i.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 • N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 . N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 ■■ N.D. 28) Naphthalene 15.37 128 304 N.D. 2 9) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 . N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 d N.D. 45) Diethylphthalate 22.11 149 101 : N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 . N.D. 47) Fluorene 0.00 166 0 ,N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 . . N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0-; N.D. -5-1-)—N -Nitro s odiphenylamine-------0.0 0 —-16 8 ----- —NtD^— 52) 4-Bromophehyl-phenylether 0.00 248 0 ■■ N.D. 53) Hexachlorobenzene 0.00 284 0. . N.D. 54) Pentachlorophenol 0.00 266 d /'■ . N.D. 55) Phenanthrene 25.02 178 575 N.D. 56) Anthracene 25.02 178 575 N.D. 57-)--Di-n-butylphthalate —----- —27.03 149- -3631— - —N-D------ 58) Fluoranthene 0.00 2 02 0 : N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 ' N.D. -61-1-Benzidine— - —- -- ------ -- -.. OvOO' _--184“ —N7D7— '6'3)~Pyrene O' .'O'O 2”0"2 N\D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.06 228 2 021, N.D. -6;6-)-Bi-s-(-2-ethylhexyl-)'phtha'la'te' —3'3T32—1’4'9“ '2157 ' NTD":: 67) Chrysene 33.06 228 2021 - . N.D. 69) Di-n-Octylphthalate 35.08 149 2 96 ; N.D. 70) Benzo(b)fluoranthene 0.00 252 0 \ N.D.

(#) = qualifier out of range (ra) = manual integration 23833.D NP101901.M Wed Oct 31 12:27:43 2001 Page 2

NYC-WTC_000089464

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NYC-WTC_000089464Source: NYC Law Department, mirrored locally

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