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GC/MS analysis results for sample AD23833, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089461–000089475

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00. MS Integration Params: RTEINT.P Quant Time: Oct 31 12:27 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901 V

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 521140 . 20.00 ug/1 -0.04 19) Naphthalene-d8 15.32 136 2025892 20.00,ug/1 -0.04 31) Acenaphthene-dlO 20.60 164 965238 20.00 ug/1 -0.03 49) Phenanthrene-dlO 25.02 188 13658'90 . 20.00 ug/1 -0.04 59) Chrysene-dl2 33.06 240 859733 20.00 ug/1 -0.04 68) Pery-lene-dl2 37.15 264 606667 20.00 ug/1 -0.04. System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.71 132 3 03 0.01 ug/1 0.45 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.24 152 5354 0.15 ug/1 -0.03 Spiked Amount 50.000 Recovery = 0.30% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.75 172 1879 0.02 ug/1 0.09 Spiked Amount 50.000 Recovery = , 0.04% 33) 2,4,6-Tribromophenol 0.00 330 ■ 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 62) Terphenyl-dl4 0.00 244 .0 0.00 ug/1 Spiked Amount 50.000 Reedvery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 , 0/. N.D. 8) Phenol 0.00 94 0. N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. —-10)- 2-Ghlorophenol— 0.00 -128 _0- N.D.- 11) 1,3-Dichlorobenzene 0.00 146 ■ 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. —1'3)- -1, 2 -Dichlorobenzene--- “0“00---146---- ' ; O" N.7D<: 1“4)" 2-Me'tHyipHeri61 ~ “dTd-cf *1 os- 0 N.D."" 15) 2,2'-oxybis(1-Chloropropan 0.00 45 . 0 N.D. 16) 3&4-Methylphenol 0.00 108 ‘ d N.D. 17) N-Nitfb'sd'^di~h"pfdpyiaMn^ OTOK •70’■r NTD” 18) Hexachloroethane 0.00 117 .0 N.D. 21) Nitrobenzene 0.00 77 - ' 0 •; N.D. 22) Isophorone 0.00 82 0. N.D. (#) = qualifier out of range (m) = manual integration 23833.D NP101901.M Wed Oct 31 12:27:39.2001 Page 1

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