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GC/MS analysis results for sample AD23651, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.

NYC-WTC_000089059–000089072

Folder label: “GC/MS Scan 9/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\23651.D Vial: 5 Acq On : 15 Oct 2001 4:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 15 16:55 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE. Integrator) Title : 209' 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response. Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 15.43 128 123 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 2 0.97 165 272 N.D. 45) Diethylphthalate 22.16 149 2637 N. D .- 46) 4-Chlorophenyl-phenylether 0.00 204 0 . N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 'N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0- N.D. --- 51-)—N-Nitrosodiphenylamine —— -O-.-OO- -168- -T—N-D- 52) 4-Bromophenyl-phenylether 0.00 248 0 . N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 .. 0 N.D. 5 5) Phenanthrene 25.10 178 346 N.D. 56) Anthracene 25.10 178 346. N.D. 57) Di-n-butylphthalate 2.7_.,08_149_ -__ 3352^ _N..D.- - --58) Fluoranthene 0.00- 202 ' 0 N.D. __ _ 60) 3,3' -Dichlorobenzidine. . „0..00_252 0 --N-.D. ^^61.)—Benz idine r——2---- —--- ^0.;.;00^184-— -;-0.— -^N^-D— ■——6-3~-)—Pyrene'—"—------ ~ =0t0’0'=-2'0'2'=‘ ■—O'— -- NTDT 64) Butylbenzylphthalate 0.00 149 -0 . N.D. 65) Benzo(a)anthracene 33.13 228 2365_., N.D. —66-)—Bi-s-(-2-ethy-lhexyI-) phthalate-—3-3—3-9- -149 ■29&6-tr NTD— 67) Chrysene ' 33.'13 228 2365 N.D. 69) Di-n-Octylphthalate 0.00 149 0 ‘ N.D. 70) Benzo(b)fluoranthene 0.00 252 Oa: . . N.D. (#) = qualifier out of range (m) = manual integration . 23651.D NP091101.M Tue Oct 16 09:39:02 2001 . Page 2

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