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GC/MS analysis results for sample AD23651, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23651 conducted on October 16, 2001.

NYC-WTC_000089059–000089072

Folder label: “GC/MS Scan 9/28/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1501\23651.D Vial: 5 Acq On : 15 Oct 2001 4:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1,00 MS Integration Params: RTEINT.P Quant Time: Oct 15 16:55 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.76 152 588018 20.00 ug/1 -0.15 19) Naphthalene-d8 15.38 136 2310601 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 1100863 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.09 188 1566868 20.00 ug/1 -0.15 ' 59) Chrysene-dl2 33.13 240 1087397 20.00 ug/1 -0.15 68) Perylene-dl2 37.24 264 803141 20.00 ug/1 -0.18. . System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.28 152 5890 0.21 ug/1 -0.15 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.81 172- 2463 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. _ul0-)_2--Chlorophenol ----- —-———0.0 0—12 8— -0- -- NtDi-- 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) _1,, 4-Dichlorobenzene----- 0.00 146-- — -0 N-.D. - —1-39—1—2 - D ich-lor ohen z ;------- 0 -0 0 —14 6-±-Tr -0- =^l-4-)‘^2^Methylphenel----------------- ------------ 0T0'0“l*0'8------ "0~ ^ntd: 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16)_ 3&4-Methylphenol_____ 0.00^108 0 . N,.D.__ J. —i7)-^N=Nitroso—di—n-propyl'amine' — 07‘00~='^70“— “0“ •~N7DT7T“ 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 23651.D NP091101.M Tue Oct 16 09:38:57 2001 Page 1

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