GC/MS scan page fragment from September 27, 2001

NYC 9/11 Public Portal Document LSC Area Percent Report 1 File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 on : 16 Oct 2001 4:11 pm Operator: 2 09 GTkLOS JSple lab blk ,9/27 Inst : GC/MS 209 Mise ' . Multiplr: 1.00 US Integratxon Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP09110 (RTE Integrator) Title : 209 625/TCLP calibration ta'Me 7/16/01 Smoothing : OFF Y Filtering: 5 Sampling : 1 A, Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailin Peak separation: 5 T 101) prefer < Baseline drop else tangent >

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.131 7 10 18 rVB2 11356 26888 1.00% 0.165% 2 6.370 142 145 152 rBV 20765 43637 1.63% 0.268% 3 6.480 152 157 166 rW 35132 87989 3.28% 0.540% 4 6.609 168 171 18 0 rW 16826 37126 1.39% 0.228% 5 6.728 180 184 191 rW 23214 49054 1.83% 0.301%

6 7.205 229 236 241 rBV 10745 31703 1.18% 0.194% 7 11.621 712 717 724 rBV 22116 49616 1.85% 0.304% 8 11.759 727 732 751 rW 791822 1916650 71.51% 11.756% 9 15.376 1119 1126 1143 rBV 1100089 2592602 96.73% 15.901% 10 20.654 1694 1701 1716 rBV 1223805 2680117 100.00% 16.438% 11 25.079 2177 2183 2196 rBV2 1130618 2484855 92.71% 15.241% 12 29.504 2659 2665 2672 rBV 75694 153162 5.71% 0.939% 13 29.624 2672 2678 2686 rVB 42800 85199 3.18% 0.523% 14 29.752 2686 2692 2700 rBV2 18982 40044 1.49% 0.246% 15 30.707 2789 2796 2802 rBV 65836 134616 5.02% 0.826% 16 31.643 2892 2898 2903 rBV 61677 123027 4.59% 0.755% I 17 31.735 2903 2908 2917 rW 130497 273561 10.21% 1.678% 18 32.727 3011 3016 3029 rBV 121703 276601 10.32% 1.697% 19 33.121 3052 3059 3077 rBV2 914038 2140886 79.88% 13.131% 20 33.691 3113 3121 3133 rBV 143112 321477 11.99% 1.972%

21 34.609 3216 3221 3231 rBV 100199 225166 8.40% 1.381% 22 35.499 3309 3318 3329 rBV 78692 . 201579 7.52% 1.236% 23 36.362 3406 3412 3424 rBV2 39441 120073 4.48% 0.736% 24 37.234 3498 3507 3526 rBV2 660764 1954621 72.93% 11.988% 25 38.363 3622 3630 3638 rBV6 8589 37962 1.42% 0.233%

26 39.731 3772 3779 3788 rVB5 8289 38546 1.44% 0.236% 27 41.705 3981 3994 4004 rBV4 12997 83064 3.10% 0.509% 28 44.174 4252 4263 4265 rBV5 12029 50211 1.87% 0.308% 29 47.314 4593 4605 4606 rBV5 10586 44174 1.65% 0.271%

Sum of corrected areas: 16304206

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