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GC/MS analysis results for sample AD22777, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22777 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087953–000087972

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document Liinrary aearcn Compound Report Data File C:\HPCHEM\1\DATA\OCT0401\22777.D Vial: 8 Ac'q On 4 Oct 2001 10:23 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanol, 4-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.45 ug/1 66124 1,4-Dichlorobenzene-d4 11.78

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol -methyl- 102 C6H14O 000108-11-2 83 2 2-Hexanol/ 102 C6H14O 000626-93-7 83 3 2-Butanol 74 C4H10O 000078-92-2 50 4 2-Hex^l, (S)-__________________ 102 C6H14O 052019-78-0 43 Abundance Scan 184 (6.733 min); 22777.D (-) Wz 44.95 100.00% 4)5

5000

. . I . r ■. p . I . . I . . I 41 69 53^6 I 84 87 6.40 6.60 6.80 7.00 i"'l|........ . ......... .................... m/z 69700 15773% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546; 2-Pentanol, 4-methyI- 4^

.......... k ............. 6.40 6.60 6.80 7.00 27 m/z 41.05 12.48% 69 19 I 31 4: 5,7 1 8487 .......... . .............................................. ... TT/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 f\bundance #63582:2-Hexanol 4|5 .. I .... I .... I , 6.40 6.60 . 6.80 7.00 553 m/z 43.95 10.01%

27

Tl/Z-> rp- I‘ 19 'I 3* . .................. . 31 ........... '' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ......... . 8487

Abundance #62568: 2-Butanol —• I I III > I . . . . ■] I I . . I . I ' ' r 4)5 6.40 6.60 6.80 7.00 m/z 43.00 9.98%

Ti/z-> 5000

10 27 31

15 20 25 30 35 40 45 59

50 55 60 65 72 '''' I 70 75 80 85 90 95 I'''' I r JVJ 6.40 L_ 6.60 6.80 7.00

22777.D NP091101.M Fri Oct 05 12:49:08 2001 Page 2

NYC-WTC_000087961

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