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GC/MS analysis results for sample AD22976, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22976 conducted on October 15, 2001, identifying unknown compounds.

NYC-WTC_000087863–000087874

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document yuancicacxon Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1101\22976.D Vial: 7 Acq On : 11 Oct 2001 3:37 pm Operator: 209 GALOS Sample -. reinject Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 11 16:25 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Thu Sep 13 12:47:04 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 17.24 107 580 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 18.92 162 102 N.D. 38) Dimethylphthalate 20.02 163 814 N.D. 39) 2,6-Dinitrotoluene 20.24 165 985 N.D. 40) Acenaphthylene 20.19 152 1598 N.D. 41) Acenaphthene 20.75 153 1367 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 21.42 165 1394 N.D. 45) Diethylphthalate 22.16 149 4073 N.D. 46) 4-Chlorophenyl-phenylether 22.31 204 766 N.D. 47) Fluorene 22.26 166 2878 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 22.76 77 2403 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 22.69 168 1551 N.D. 52) 4-Bromophenyl-phenylether 23.76 248 359 N.D. 53) Hexachlorobenzene 24.17 284 968 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.15 178 5176 N.D. 5 6) Anthracene 25.27 178 10521 N7iyT> 57) Di-n-butylphthalate 27.08 149 58673 0.53 ug/1 99 58) Fluoranthene 28.76 202 6107 n.d/ 60) 3,3'-Dichlorobenzidine 33.10 252 1145 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 29.43 202 6472 N.D. 64) Butylbenzylphthalate ' 31.59 149 4081 N.D. 65) Benzo(a)anthracene , 33.07 228 9434 N.D. 66) Bis(2-ethylhexyl)phthalate 33.38 149 11229 N.D. 67) Chrysene 33.07 228 9434 N.D. 69) Di-n-Octylphthalate 35.12 149 9179 N.D. 70) Benzo(b)fluoranthene 36.13 252 7041 N.D.

(#) = qualifier out of range (m) = manual integration 22976.D NP091101.M Mon Oct 15 08:39:06 2001 Page 2

NYC-WTC_000087866

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NYC-WTC_000087866Source: NYC Law Department, mirrored locally

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