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GC/MS analysis results for sample AD23079, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD23079 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087794–000087816

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Dat,a File C:\HPCHEM\1\DATA\OCTO 3 01\23079.D Vial: 6 Acq On 3 Oct 2001 5:32 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.384 140 146 153 rBV 21312 51826 1.49% 0.268% 2 6.485 153 157 167 rW 32458 92539 2.67% 0.478% 3 6.622 168 172 179 rW 17840 43213 1.25% 0.223% 4 6.732 180 184 197 rVB 23349 57731 1.66% 0.298% 5 11.644 714 719 728 rVB 27526 65069 1.88% 0.336%

6 11.782 728 734 754 rVB 1025942 2516926 72.56% 12.992% 7 1121 1128 1145 rBV 1565164' 3447019 99.37% 17.793% 8 2Cr>€J7 1697 1703 1715 rBV 1546669 3468748 100.00% 17.905% 9 2179 2186 2198 rBV2 1485370 3189840 91.96% 16.466% 10 ■^^^^^^2399 2403 2408 rBV 43365 81387 2.35% 0.420%

11 29.536/2662 2668 2674 rBV 82061 163085 4.70% 0.842% 12 29.6470,2674 2680 2684 rBV 23364 42249 1.22% 0.218% 13 30.730^/ 2791 2798 2804 rVB 34482 68638 1.98% 0.354% 14 31.666^2895 2900 2905 rBV2 70561 132287 3.81% 0.683% 15 31.758/2905 2910 2918 rVB 69376 140557 4.05% 0.726% \/ 3012 3019 3028 rBV 16 32.759 69039 142091 4.10% 0.733% 17 3054 3062 3076 rBV2 1190678 2776829 80.05% 14.334% 18 33.713 3114 3123 3135 rBV 82922 174850 5.04% 0.903% 19 34.631 y 3219 3223 3230 rVB 56959 121156 3.49% 0.625% 20 35.522 y 3312 3320 3330 rBV 50488 114387 3.30% 0.590% 36.385\/ 3409 3414 3423 rBV3 21 26922 66849 1.93% 0.345% 22 3502 3510 3527 rBV2 829972 2415515 69.64% 12.469%

Sum of corrected areas: 19372791

23079.D NP091101.M Tue Oct 09 09:57:18 2001

NYC-WTC_000087799

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