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GC/MS calibration data for TCLP method, Oct 2001

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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.

NYC-WTC_000087659–000087669

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C;\HPCHEM\1\DATA\OCT0201\22775.D Vial: 12 Acq On : 3 Oct 2001 12:52 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 t Min Area: 1 % of larges.t Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.369 141 145 149 rBV 21019 42650 1.23% 0.236% 2 6.470 153 156 160 rBV 30357 63374 1.83% 0.351% 3 6.607 168 171 180 rVB 15941 37788 1.09% 0.209% 4 6.727 180 184 190 rBV 23531 49054 1.42% 0.272% 5 11.647 715 720 729 rVB 25117 64256 1.85% 0.356% 6 729 735 751 rBV 909676 2426333 70.00% 13.446% 7 15.402 1122 1129 1147 rBV 1562793 3340080 96.37% 18.510% 8 2-0..£ai' 1698 1704 1725 rBV 1603159 3466045 100.00% 19.208% 9 2180 2187 2197 rBV 1475290 3167351 91.38% 17.553% 10 3055 3063 3081 rBV2 1190082 2856760 82.42% 15.831% 11 33.>2ia 3502 3511 3524 rBV2 859747 2531117 73.03% 14.027%

Sum of corrected areas: 18044808 22775.D NP091101.M Thu Oct 04 10:46:47 2001

NYC-WTC_000087663

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NYC-WTC_000087663Source: NYC Law Department, mirrored locally

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