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GC/MS analysis results for sample AD22918, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22918 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087599–000087622

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087607
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0 2 01\22918.D Vial: 8 Acq On 2 Oct 2001 8:57 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.48 0.66 ug/1 75853 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-He:}C .one 100 C6H12O 000591-78-6 91 2 Oxir^.ne, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 3 2-Xexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 50 4 l^thyl I sotjutyl Ketone 100 C6H12O 000108-10-1 47 ^bugrfance Scan 157 (6,480 min); 22918.D (-) m/z 42.95 100.00% 43

58 5000

6.20 6.40 6.60 6.80

■Ti/z-> 20 30 440 ' I ' ' ' ' I ' 50 60 71 70 80 85 90 100 100 110 120 130 140 m/z 58.05 54.78% Abundance #63384; 2-Hexanone. 43

553 58 6.20 6.40 6.60 6.80 29 "m/z 41.05 15.30%

Tife-> 20 LX 30 40 50 60 71 70 80 85 90 IM 100 110 120 130 140 Abundance #1530; Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 6.20 6.40 6.60 6.80 5000 ■m/z 57.00 ■ 12.72% 71

30 85 100 11111,, 11.1,1 r I''' ‘ I'''' I'''' I' Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyl- 43 6.20 6.40 6.60 6.80 m/z 100.05 9.38% 58

Tl/Z~> 553 29

' I'' ''I''''II 20 30 40 'ir ' ' 50 ,1 60 71

70 80 85

90 100 110 120 130 140 140 6.20 k 6.40 A 6.60 6.80

22918.D NP091101.M Thu Oct 04 09:42:39 2001 Page 2

NYC-WTC_000087607

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NYC-WTC_000087607Source: NYC Law Department, mirrored locally

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