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GC/MS analysis results for sample AD22654, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22654 conducted on October 12, 2001, noting other unknown compounds.

NYC-WTC_000087463–000087490

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\HPCHEM\1\DATA\OCT1101\22654.D vial: 6 , Acq On : 11 Oct 2001 2:38 pm Operator: 209 GALOS Sample : reinject Inst : GC/MS 209 ' Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* I Peak Number 17 Tetratetracontane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 38.36 1.10 ug/1 149970 Perylene-dl2 37.23 1 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratetracontane 619 C44H90 007098-22-8 91 1 2 Docosane 310 C22H46 000629-97-0 91 3 Nonadecane 268 C19H40 000629-92-5 90 4 Heptadecane 240 C17H36 000629-78-7 90 Abundance Scan 3629 (38.359 min); 22654.D (-) ^m/z SYTOO 100.00% 5/ I

I 85 5000

38.00 38.20 38.40 38.60 J 253282 m/z 71.05 76.90% '' I' •n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068; Tetratetracontane 57

5000 85 38.00 38.20 38.40 38,60 m/z43.05 63.86% ]_ I I H^ri''^\''?Q197225 379407 590618 Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance ' #44318; Docosane 57

85 38.00 38.20 38.40 38.60 5000 m/z 85.00 51743%

. 266 310 .......................... ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #71949; Nonadecane 57 38.00 38.20 38.40 38.60 "m/z 55.00 26758% 5000 85

|113 ,141169 224268 ' f T' ' ' ' I mfe-> 50 100 150 200 250 300 350 400 450 500 550 600 38.00 38.20 38.40 38.60

I I

22654.D NP091101.M Fri Oct 12 09:09:39 2001 Page 17

NYC-WTC_000087488

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NYC-WTC_000087488Source: NYC Law Department, mirrored locally

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