NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\SEP2801\22652 .D Vial: 11
Acq On : 28 Sep 2001 10:14 pm Operator: 209 GALOS
Sample : gc/ms unknown Inst : GC/MS 209
Mise Multiplr; 1.00
MS Integration Params; LSCINT.P
Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library ; C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 18 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
41.79 2.23 ug/1 319969 Perylene-dl2 37.29
Hit# of 5 Tentative.-ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4, X7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 37
2 Oxazole, .iphenyl- 221 C15H11NO 004675-18-7 14
3 Trisilox. Jie, 1,1, 1,5,5,5-hexamethyl 384 C12H36O4Si5 003555-47-3 12
4 TrichJ.erfiomethyl 9-anthracenecarbodi 370 C16H9C13S2 091631-91-3 10
Abundance Scan 4003 (41.787 min): 22652.D (-) m/z 73.00 100.00%
73
147
221
5000
281
429 4140 41.60 41.80 42.00 42.20
42 25^
' I' •" I" " I" •' I m/z 147.00 6^747%
nfe-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoclane, 2,2,4,4,5,5,7,7-
147 2;l
73
5000
41.40 41.60 41.80 42.00 42.20
191 m/z 221.00 56.76%
117 279
I I ""I ""If"" I ""I
I" " I "' ‘T' ‘" I " ’ ‘ 1
■n/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #70577: Oxazole, 4,5-diphenyl-
2il
......
165 193 41 40 41.60 41.80 42.00 42.20
5000 m/z 281.00 27.59%
51 89
I < 1111'l 11 fl 111 I I I 111
I" " I'"' I" " I" " I
40 60 80 100120140160180200220240260280300320340360380400420
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 41.40 41.60 41,80 42.00 42.20
147 m/z 355.00 23.92%
553
281
45 369 ...................
IJ, , , [........ 117 .... ,........ .... 249 ,.................... ...... 1[...................
tnZz-> 40 60 80 100120140160180200220240260280 300 320 340 360 380 400 4^ ' 41.40 41.60 41.80 42.00 42.20
22652.D NP091101.M Wed Oct 03 11:53:40 2001 Page 18
NYC-WTC_000087298
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