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ICP-MS Daily Performance Check, Jan 17 2002

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Laboratory record of daily instrument tuning and performance verification for ICP-MS on January 17, 2002.

NYC-WTC_000086557–000086558

Folder label: “ICP-MS Tuning & Optimization Information

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NYC 9/11 Public Portal Document

Daily Performance Report Sample ID: DPC Sample Date/Time: Thursday, January 17,2002 08:55:23 Sample Description: DAILY PERFORMANCE CHECK Method File: d:\elandata\Method\Daily.mth Dataset File: d:\elandata\Dataset\daily performance\DPC.2249 Tuning File: d:\elandata\Tuning\default.tun Optimization File: d:\elandata\Optimize\default.dac Dual Detector Mode: Pulse Acq. Dead Time(ns): 55 Current Dead Time (ns): 55

Summary Analyte Mass Meas. Intens. Mean Net Intens, Mean Net Intens. SD Net Intens. RSD Mg 24.0 74408.3 74408.274 262.617 0.4 Rh 102.9 354367.2 354367.171 1186.560 0.3 In 114.9 486123.3 486123.265 1454.459 0.3 Pb r> Ba 208.0 137.9 336997.6 424113.4 336997.569 424113.439 J 1524.396 1293.935 0.5 0.3 L Ba++ 69.0 4785.0 0.011 J 0.000 . 0.6 r> Ce 139.9 517429.3 517429.286 1571.140 0.3 L CeO 155.9 15196.2 y 0.029 J 0.000 0.7 Bkgd 220.0 17.834 2.051 11.5

Current Optimization File Data Current Value Description 0.89 Nebulizer Gas Flow 6.25 Lens Voltage 1000.00 ICP RF Power -1887.50 Analog Stage Voltage 1500.00 Pulse Stage Voltage 70.00 Discriminator Threshold -6.00 AC Rod Offset 60.00 Service DAC 1 0.00 Quadrupole Rod Offset

Current Autolens Data Analyte Mass Num of Pts DAC Value Maximum Intensity Be 9 21 5.8 7558.2 Al 27 21 6.0 179221.1 Sc 45 21 6.0 1010866.2 V 51 21 6.0 222947.9 Cr 52 21 6.3 202078.3 Mn 55 21 6.3 303423.5 Ni 58 21 6.0 128259.7 Co 59 21 6.3 223383.4 Cu 63 21 6.0 116913.1 Zn 64 21 6.3 63718.2 Cu 65 21 6.5 57939.6 Zn 66 21 6.3 38135.2 Zn 68 21 6.3 27276.1 Ge 74 21 6.5 265184.8 As 75 21 6.3 34129.3

Sample ID: DPC Report Date/Time: Thursday, January 17, 2002 08:58:49 Page 1

NYC-WTC_000086557

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NYC-WTC_000086557Source: NYC Law Department, mirrored locally

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