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ICP-MS daily performance check, Jan 07 2002

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Laboratory report of ICP-MS instrument tuning and daily performance verification on January 7, 2002.

NYC-WTC_000086539–000086540

Folder label: “ICP-MS Tuning & Optimization Information

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NYC 9/11 Public Portal Document

Daily Performance Report Sample ID: DPC Sample Date/Time: Monday, January 07, 2002 10:16:30 Sample Description: DAILY PERFORMANCE CHECK Method File: d:\elandata\Method\DAILY PERF TO SAVE REPORT.mth Dataset File: d:\elandata\Dataset\daily performance\DPC.1762 Tuning File: d:\elandata\Tuning\default.tun Optimization File: d:\elandata\Optimize\default.dac Dual Detector Mode: Pulse Acq. Dead Time(ns): 55 Current Dead Time (ns): 55

Summary Analyte Mass Meas. Intens. Mean Net Intens. Mean Net Intens. SD Net Intens. RSD Mg 24.0 58250.1 58250.097 . 396.383 0.7 Rh 102.9 295857.1 295857.129/ 2748.314 0.9 In 114.9 390269.4 390269.357 , 4011.827 1.0 Pb 208.0 231914.7 231914.720 / 1531.232 0.7 r> Ba 137.9 328975.2 328975.185 2229.476 0.7 L Ba++ 69.0 5502.4 0.017 J 0.000 0.3 r> Ce 139.9 410488.4 410488.370 3954.718 1.0 L CeO 155.9 11990.7 0.029 0.000 0.8 Bkgd 220.0 11.0 / 11.033 1.673 15.2

Current Optimization File Data Current Value Description 0.89 Nebulizer Gas Flow 6.25 Lens Voltage 1000.00 ICP RF Power -1825.00 Analog Stage Voltage 1400.00 Pulse Stage Voltage 70.00 Discriminator Threshold -6.00 AC Rod Offset 60.00 Service DAC 1 0.00 Quadrupole Rod Offset

Current Autolens Data Analyte Mass Num of Pts DAC Value Maximum Intensity Be 9 21 5.8 5221.6 Al 27 21 5.5 116685.2 Sc 45 21 5.8 646172.8 V 51 21 6.3 141656.5 Cr 52 21 6.5 124214.1 Mn 55 21 6.3 191916.5 Ni 58 21 6.0 89125.6 Co 59 21 6.0 153710.1 Cu 63 21 6.0 80757.9 Zn 64 21 5.8 41093.1 Ge 74 21 6.3 168794.3 As 75 21 6.5 23771.3 Se 82 21 6.3 3230.6 Mo 98 21 6.0 79799.5 Ag 107 21 6.5 132073.8

Sample ID: DPC Report Date/Time: Monday, January 07, 2002 10:19:56 Page 1

NYC-WTC_000086539

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NYC-WTC_000086539Source: NYC Law Department, mirrored locally

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