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Method 200.8 ICP-MS lab results, NEWE samples, Jan 11, 2002

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ICP-MS analysis of water samples using Method 200.8 with elemental measurements (Be, Sc, Mn, In, Sb, Ho) and quality control replicates performed on January 11, 2002.

NYC-WTC_000085478–000085537

Folder label: “NEWE 1/11/2002 AD 31456 - AE00110 Batches 16390 16391 16402 copies made

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NYC 9/11 Public Portal Document

Method 200.8 - Summary Report Sample ID: AD31550 Sample Date/Time: Friday, January 11, 2002 13:34:21 Sample Type: QC Duplicate Sample Description: Number of Replicates: 3 Batch ID: Method File: d:\elandata\Method\NEWE200.8.mth Dataset File: d:\elandata\Dataset\daily performance\AD31550.2042 Sample Prep Volume (mL): Initial Sample Quantity (mg): Aliquot Volume (mL): 5e+001 Diluted To Volume (mL): 1e+002

Concentration Results Analyte Mass Meas. Intens. Mean Meas. Intens. RSD Net Intens. Mean Cone. Mean Cone. RSD Sample Unit r Be 9 12.000 22.048 0.000 0.00526 226.25 ug/L |> Sc-1 45 604289.618 4.805 604289.618 ug/L L Mn 55 289529.771 1.857 0.479 33.20330 5.13 ug/L r> In 115 1287098.498 1.147 1287098.498 ug/L I Sb 121 367.344 3.011 0.000 0.08027 3.61 ug/L L Sb 123 293.560 3.405 0.000 0.08414 4.53 ug/L r> Ho 165 1749485.888 3.022 1749485.888 ug/L L Tl 205 277.340 9.294 0.000 0.00488 31.33 ug/L

QC Calculated Values Analyte Mass QC Std % Recovery Int Std % Recovery Spike % Recovery Dilution % Diff Dup. Rei. % Diff r Be 9 722.645 |> Sc-1 45 95.172 L Mn 55 r> In 115 97.598 I Sb 121 7.152 L Sb 123 2.617 r> Ho 165 97.408 L Tl 205 41.415 Calibration Analyte MassCurve Type Correlation Coefficient r Be 9Linear Thru Zero 0.999992 |> Sc-1 45Linear Thru Zero L Mn 55Linear Thru Zero 0.999983 r> In 115Linear Thru Zero I Sb 121 Linear Thru Zero 0.999998 L Sb 123Linear Thru Zero 1.000000 r> Ho 165 Linear Thru Zero L Tl 205Linear Thru Zero 0.999977

Sample ID: AD31550 Report Date/Time: Friday, January 11,2002 13:34:54 Page 1

NYC-WTC_000085507

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