VOC analysis results, sample AE12531, May 2002

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Data File C:\HPCHEM\l\DATA\02may24\12537.D Vial: 3 Acq On 24 May 2002 11:51 pm Operator: 201-wb Sample 524 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration ParamsLSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peale Number 3 Cyclotetrasiloxane, octamethyl Concentration Ranle 2

R.T. EstConc Area Relative to ISTD R.T. 22.70 0.07 ug/L 71935 CHLOROBENZENE-D5 21.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 4 3 7a,9c-(Iminoethano)phenanthro[4,5-b 281 C18H19NO2 024695-70-3 4 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 3 Abundance Scan 1099 (22.695 min); 12537.D (-) m/z 281.25 100.00% 21(1

5000

73 133 22.40 22.60 22.80 23.00 45 I I 191 207 249 265 m/z 282.35 36.44% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 2$1

wiilil 22.40 22.60 22.80 23.00 m/z 283.35 23.73% 133 207 73 I 16317719J I 235249 265 « I i ' I I ' ' V ' I «'I* I ' ' ' i' '' ' 1' ' '' I tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 2)!1

22.40 22.60 22.80 23.00 5000 m/z 73.05 18.68%

__ 253 126 203 I I J.^2242^dUL m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39622: 7a,9c-(lminoethano)phenanthro[4,5-bcd]furan, 4a.alp 2$1 22.40 22.60 22.80 23.00 m/z 133.15 14.11% 253 5000 165 209 181 „„,238 151 224

I'''' I' ‘' I iVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 22.40 22.60 22.80 23.00

12537.D HP051702.M Sat May 25 00:31:22 2002 Page 3

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