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VOC analysis results, sample AE11409, May 2002

Machine-extracted title · confidence 95%

Laboratory report for volatile organic compounds in sample AE11409 analyzed on May 16, 2002.

NYC-WTC_000083201–000083263

Folder label: “524 5/11/02

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Scanned page image, NYC-WTC_000083232
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\5973N\02MAY16\11409 .D Vial: 8 Acq On 16 May 2002 4:24 pm Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P

Quant Method : C:\MSDCHEM\1...\W042302.M (RTE Integrator) Title . : VOC method 8260 Library : C:\DATABASE\WILEY7N.L

Peak Number 3 Cyclotrisiloxane, hexamethy... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 21.15 0.08 ug/L 39298 1,4-Difluorobenzene 17.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotrisiloxane, hexamethyl- $$... 222 C6H18O3Si3 000541-05-9 78 2 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 74 3 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 64 4 Cyclotrisiloxane, hexamethyl- 222 C6H18O3Si3 000541-05-9 64 Abundance Scan 1754 (21.150 min): 114O9.D(-) m/z 207.00 100700% 207

5000 96 A AA a^-ZiA, I <1 , , I 7

41 50 77 119 133 177 191 20.80 21.00 21.20 21.40 0 P*'. ....... . I" I 11 I • " • I • " • I I"''' I '''' I'' m/z 97770 27727% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 (Abundance #146392: Cyclotrisiloxane, hexamethyl- $$ Dimethylsiloxane... 207

5000 20.80 21.00 21.20 21.40 m/z 208.00 77733% 87 I , 119 147 163 177 Ifl 0^ I ' ' '''l • ' I ' I i'l ■ ' I " I'"I''"I' I " " l'''' ' . I .... I ... . I I'. . I I r , 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 (\bundance #146396: Cyclotrisiloxane, hexamethyl- 207 T 20.80 21.00 21.20 21.40 5000 m/z 209.10 15777%

75 T 119 ^33 ,63 I 0 I' " ' I'''' I * " ' I rTi i p. n I I I I r. I I'l I . I I .’| I t I . I < I I < I. . II... . I .... I ... > I r.. . I J mfe-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 (\bundance #146391: Cyclotrisiloxane, hexamethyl- 2(17 2030 21.00 21.20 21.40 m/z 133.10 9.83%

5000

96 I , 119 147 163 177 1^1 I 0 p-TlVpS-rrp-rTTYrTTTp.tTTp-rTVp-r-rTj-iVT-rp-rtV|-i-nr^^ L Tl/Z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 20.80 21.00 21.20 21.40

11409.D W050302.M Fri May 17 14:27:33 2002 Page 5

NYC-WTC_000083232

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