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GCMS analysis results for sample AE11422, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11422 conducted on May 30, 2002.

NYC-WTC_000025464–000025478

Folder label: “GCMS X 5/16/02 A 5/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052002\11422.D Vial: 12 Acq On : 20 May 2002 10:14 pm Operator: Mclean Sample : 5/16 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 Cyclotrisiloxane, hexamethyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.38 0.21 ug/L 120044 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-9 39 2 Cyclotrisiloxane, hexamethyl- 222 C6H1803Si3 000541-05-939 3 N-(2-Acetylcyclopentylidene)cycl ... 207 C13H21NO 1000100-48-5 9 4 2-Ethylacridine 207 C15H13N 1000147-64-9 9 Abundance Scan 392 (5.382 min): 11422.D (-378) (-) m/z 207.00 100.00% 207

5000

51 96 86 5.00 5.20 5.40 5.60 5.80 0J । । । । । । । , , 40 hl 1 _______ L 1 1 1 I1 1 ' ‘1 1 1 ' ' 1 1 11. m/ Z 2 0 8.00 23.76% miz-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84874: Cyclotrisiloxane, hexamethyl- 207

5000 5.00 5.20 5.40 5.60 5.80 96 m/z 95.90 17.46% 191 4 15 29 45 61 75 85. | , 11,9 133 147 163 177 0- TTn———m. 11 I, I’r’II * — i ■ ■ 1 '■ i 1 1 III* TI ""I m/z-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #126480: Cyclotrisiloxane, hexamethyl- 207

500 5.20 5.40 5.60 5.80 5000 m/z 87.90 17.38%

96 28 45 61 133 147 163 177 191 75.86 . 106 119 1 .A 0 IIII1*1**I7* 'i 1 11 i 1 1 1 |T 1 ' ‘ii r 14 , H—r 1IT n/z-> 0 20 40 60 80 100 120 140 160 180 200 Abundance #84801: N-(2-Acetylcyclopentylidene)cyclohexylamine 207 5.00 5.20 5.40 5.60 5.80 164 m/z 51.00 15.63% 124 5000 41 55 67 82 97 110 150 192 "M"MMMMw-Wap, . | , J II! J I | ! | , I II [l I , I 136 । 178

n/z—> 0 0 1 1 ' 1 1 1 1 20 40 60 80 100 120 — . ,1 . ! 140 160 I T’I 1 ' 180 200 1. 1 i ' 1 ' ■ i ■ ■ ' ■ i ' ■ ■ 1 । ■ ■ ■ ' । 1 1 5.00 5.20 5.40 5.60 5.80

11422.D 050102.M Thu May 23 10:49:08 2002 Page 6

NYC-WTC_000025474

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NYC-WTC_000025474Source: NYC Law Department, mirrored locally

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