VOC analysis results, sample AE10240, May 3, 2002

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Data File C:\MSDCHEM\l\5973N\02MAY03\10242.D Vial: 13 Acq On 3 May 2002 7:29 pm Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P

Quant Method : C:\MSDCHEM\1...\W050302 .M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 5 3,6-DIHYDRO-2H-PYRAN-2-ONE ... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 33.78 0.04 ug/L 23217 1,4-Dichlorobenzene-d4 31.54 Hit# ..of 5 Tentative ID MW MolForm CAS# Qual ------------- --------- - ------;------------------------------------------------------------------------------------------ 1 3,6-piHYDRO-2H-PYRAN-2-ONE $$ 2H... 98 C5H6O2 026677-08-7 35 2 2-Nonenal, (E)- 140 C9H16O 018829-56-6 35 3 Heptane, . 3-methylene- 112 C8H16 001632-16-2 35 4 2-Decenal, (E)- (CAS) $$ trans-2... 154 C10H18O 003913-81-3 27 Abundance > Scan 3034 (33.784 min): 10242.D (-) m/z 43710 100.00% 4& 70 55 5000 83 112 207 33 40 33.60 33.80 34.00 34.20 0 p-rrrp-rrry I 11 m/z TOTOO 67.06% Ti/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #6831: 3,6-DIHYDRO-2H-PYRAN-2-ONE $$ 2H-Pyran-2-one, 3,6-d...

39 5000 3340 33.60 33.80 34.00 34.20 98 m/z 55700 62775% oV^ 'I I " »• I " I ” " I " " I ’'' ‘ I tVz-> 20 30 40 50 60 70 80 90 100110 120130140150 160170 180190 200 210 Abundance #35994: 2-Nonenal. (E)- 43 55 70 t. J 27 83 33 40 33.60 33.80 34.00 34.20 5000 mTz 477177 60.96% 96

140 0 ' I " '' i " " I'' " I' ' I'' ‘ I'" ‘ I' " ‘ I'' Ti/z-> Abundance 20 30 40 50 60 70 80 90 100110 120130140150 160170180190 200 210 #13787: Heptane, 3-methylene- .. Il 41 55 33 40 33.60 33.80 34.00 34.20 70 m/z 57710 58.50% 5000

112 p4-rTpTTTYn-rTykTTyrTrrpTTTyTTTTpTT-Tp-rTTpTTTyrT7-r[-rxTTyr^^ 0 I" " I ■nZz-> 20 30 40 50 60 70 80 90 100110 120130140150160170 180190200 210 33.40 33.60 33.80 34.00 34.20

L0242.D W050302.M Mon May 06 12:26:22 2002 Page 7

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