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VOC analysis results, sample AE10023, April 30, 2002

Machine-extracted title · confidence 90%

Laboratory report for volatile organic compounds in sample AE10023 dated April 30, 2002.

NYC-WTC_000082619–000082776

Folder label: “524 4/30/02 - 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\5973N\02APR30\10238.D Vial: 17 Acq On 1 May 2002 3:12 am Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P

Quant Method : C:\MSDCHEM\1...\W042302 .M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N.L

Peak Number 1 (2r)-2-amino-2-methyl-3-phe... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 30.49 0.06 ug/L 31391 1,4-Dichlorobenzene-d4 31.54 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (2r)-2-amino-2-methyl-3-phenylpr... 179 C10H13NO2 017350-84-4 38 2 1-Hexanol, 2-ethyl- 130 C8H18O 000104-76-7 37 3 1-Hexanol, 2-ethyl- (CAS) $$ 2-E... 130 C8H18O 000104-76-7 35 4 1-Hexanol, 2-ethyl- (CAS) $$ 2-E... 130 C8H18O 000104-76-7 35 Abundance Scan 2700 (30.487 min): 10238.D (-) m/z 57710 100.00% 517 41 Sia 70 83 98

Tl/Z-> Abundance 0^I,,.........Uli,,,1,1.111.... il|i| 20 30 40 50 60 70 a 80 90 100110 120 130 140 150 160 170 180 m/z 30.20 30.40 30.60 30.80 41.10 61763% #84940: (2r)-2-amino-2-methyl-3-phenylpropanoic acid $$ (R... 414

5000 ........ ,>■■■,< 77.....' 84 30.20 30.40 30.60 30.80 57 m/z 47710 47794% 69

m/z-> 0 I " ..............I' JOu 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I ‘’ I 135 180 rrtn

Abundance #26914:1 -Hexanol, 2-ethyl- 57

30.20 30.40 30.60 30.80 5000 m/z 55.00 36.31% 70 83 31 42 II 98 112 .04 .... I I ' • ' I « ' ' « I " ' • I H I I I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance. #26921; 1 -Hexanol, 2-ethyl- (CAS) $$ 2-Ethylhexanol $$ 2-E... T 5t7 30.20 30.40 30.60 30.80 mTz 56700 37760% 5000 41

70 83 27

Tl/Z-> OYpr I 20 " ’ I' 30 ■ ■■

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ..... (..t.H,., 30.20 30,40 30,60 30.80

L0238.D W042302.M Thu May 02 17:17:25 2002 Page 1

NYC-WTC_000082751

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NYC-WTC_000082751Source: NYC Law Department, mirrored locally

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