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Reference standard analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 12.545 157 162 180 rBV 2319407 6001392 47.06% 7.279% 2 14.205 340 345 351 rBV4 66374 159650 1.25% 0.194% 3 15.013 431 434 440 rBV4 55682 155446 1.22% 0.189% 4 17.235 673 679 685 rBV5 67622 163868 1.28% 0.199% 5 17.462 697 704 710 rBV3 78337 173105 1.36% 0.210%

6 17.589 713 718 728 rBV 4512528 10432164 81.80% 12.653% 7 17.706 729 731 743 rVB3 237999 656654 5.15% 0.796% 8 17.951 752 758 773 rBV2 4089588 8933190 70.05% 10.835% 9 18.396 802 807 818 rVB5 100357 345970 2.71% 0.420% 10 18.550 820 824 830 rBV7 46532 147726 1.16% 0.179%

11 20.781 1066 1070 1073 rBV5 68074 146387 1.15% 0.178% 12 21.371 1127 1135 1146 rBV4 92809 325592 2.55% 0.395% 13 21.888 1187 1192 1209 rBV2 4576644 12066143 94.62% 14.635% 14 23.530 1369 1373 1378 rBV4 77869 '193998 1.52% 0.235% 15 24.065 1426 1432 1435 rBV4 95706 284503 2.23% 0.345%

16 25.788 1617 1622 1627 rBV4 49129 153714 1.21% 0.186% 17 25.979 1637 1643 1659 rBV 3225218 8772334 68.79% 10.640% 18 26.496 1690 1700 1703 rBV 60374 264387 2.07% 0.321% 19 26.759 1725 1729 1747 rBV2 4750748 12752673 100.00% 15.468% 20 28.935 1961 1969 1982 rBV 3268848 8359719 65.55% 10.139%

21 29.616 2038 2044 2069 rBV 2911964 10211836 80.08% 12.386% 22 30.314 2116 2121 2124 rBV7 49460 148126 1.16% 0.180% 23 33.607 2475 2484 2499 rBV3 255081 1599043 12.54% 1.939%

Sum of corrected areas: 82447620

10186.D 050102.M Mon May 06 14:53:38 2002 Page 1

NYC-WTC_000082553

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NYC-WTC_000082553Source: NYC Law Department, mirrored locally

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