VOC analysis results, sample AE09569, April 26, 2002

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Data File : C:\MSDCHEM\l\5973N\02APR26\0426R5.D Vial: 6 Acq On : 26 Apr 2002 3:04 pm Operator: Sample : ref 5 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Lscirit.p Quant Time: Apr 29 08:52:51 2002 Quant Results File: W042302.RES

Quant Method : C:\MSDCHEM\1...\W042302.M (RTE Integrator) Title : VOC method 8260 Last Update : Mon Apr 29 08:52:24 2002 Response via : Initial Calibration DataAcq Meth : W042302

Compound R.T. Qlon Response Cone Unit Qvalue

36) Toluene 21.82 91 1424489 5.82 ug/L 100 37) trans-1,3-Dichloropropene 22.19 75 202669 5.62 ug/L 99 38) 2-Hexanone 22.53 43 179130 21.06 ug/L 98 39) 1,1,2-Trichloroethane 22.62 97 119068 5.86 ug/L 99 40) 1,3-Dichloropropane 23.24 76 224436 6.04 ug/L 98 41) Tetrachloroethene 23.49 166 305431 5.84 ug/L 99 42) Dibromochloromethane 24.01 129 117044 5.55 ug/L 96 43) 1,2-Dibromoethane 24.54 107 100471 5.97 ug/L 99 44) Chlorobenzene 25.56 112 826196 5.74 ug/L 99 45) 1,1,1,2-Tetrachloroethane 25.64 131 213125 5.92 ug/L 99 46) Ethylbenzene 25.63 91 1711772 5.85 ug/L 99 47) P & M-Xylene 25.83 91 2687405 11.79 ug/L 99 48) o-Xylene 26.95 91 1233908 5.80 ug/L 100 49) Styrene 27.03 104 901308 5.92 ug/L 100 50) Isopropylbenzene 27.82 105 1638791 5.99 ug/L 99 52) Bromoform 27.98 173 50424 5.94 ug/L 98 53) 1,1,2,2-Tetrachloroethane 28.25 83 117802m 6.40 ug/L 55) 1,2,3-Trichloropropane 28.63 75 94325 6.43 ug/L 99 56) n-Propylbenzene 28.84 91 2119998 6.50 ug/L 100 57) Bromobenzene 29.07 77 483181 6.24 ug/L 99 58) 1,3,5-Trimethylbenzene 29.22 105 1420916 6.35 ug/L 99 ■59) 2-Chlorotoluene 29.37 91 1198882 6.42 ug/L 100 60) 4-Chlorotoluene 29.47 91 1116751 6.27 ug/L 99 61) tert-Butylbenzene 30.14 119 1265537 6.42 ug/L 99 62) 1,2,4-Trimethylbenzene 30.25 105 1460702 6.46 ug/L 100 63) sec-Butylbenzene 30.68 105 1997173 6.46 ug/L 99 64) p-Isopropyltoluene 31.00 119 1620348 6.20 ug/L 100 65) 1,3-Dichlorobenzene 31.37 146 641349 6.14 ug/L 100 66) 1,4-Dichlorobenzene 31.62 146 618864 6.14 ug/L 99 67) n-Butylbenzene 32.05 91 1589846 6.37 ug/L 99 68) 1,2-Dichlorobenzene 32.60 146 485181 6.18 ug/L 99 69) 1,2,-Dibromo-3-chloropropa 34.65 157 16846m 6.48 ug/L 70) Nitrobenzene 34.91 77 47717 99.29 ug/L 99 71) 1,2,4-Trichlorobenzene 37.42 180 308337 6.23 ug/L 99 72) Hexachlorobutadiene 37.84 225 245309 6.54 ug/L 99 73) Naphthalene 38.40 128 368479 6.51 ug/L 100 74) 1,2,3-Trichlorobenzene 39.34 180 231246 6.50 ug/L 99

(#) = qualifier out of range (m) = manual integration 0426R5.D W042302.M Mon Apr 29 11:37:35 2002 Page 2

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