VOC analysis results, sample AE10240, May 3, 2002

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Data File C:\MSDchem\l\5973N\02may03\0503R5.D Vial: 9 Acq On 3 May 2002 4:21 pm Operator: Sample ref 5 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Lscint.p Quant Time: May 03 17:03:20 2002 Quant Results File: W050302.RES

Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Last Update : Fri May 03 14:58:46 2002 Response via : Initial Calibration DataAcq Meth : W050302

Compound R.T. Qlon Response Cone Unit Qvalue

36) Toluene 21.82 91 1375202 5.16 ug/L 99 37) tj^ans-l, 3-Dichloropropene 22.19 75 179859 5.07 ug/L 99 38) 2?Hexanone 22.53 43 154841 17.94 ug/L 97 39) 1/T ,'2-Trichloroethane 22.63 97 107954 5.25 ug/L 97 40) 1,3-Dichloropropane 23.25 76 197384 5.37 ug/L 98 41) Tetrachloroethene 23.50 166 287197 5.30 ug/L 99 42) Dibromochloromethane 24.01 129 97766 4.77 ug/L 97 43) 1,2-Dibromoethane 24.54 107 87054 5.26 ug/L 100 44) Chlorobenzene 25.57 112 781441 5.04 ug/L 99 45) 1,1,1)2-Tetrachloroethane 25.63 131 192131 5.17 ug/L 99 46) Ethylbenzene 25.64 91 1655849 5.07 ug/L 100 47) P & M-Xylene 25.83 91 2590760 10.17 ug/L 100 48) o-Xylene 26.95 91 1169219 5.02 ug/L 96 49) Styrene 27.03 104 842628 4.73 ug/L 99 50) Isopropylbenzene 27.82 105 1568404 4.83 ug/L 100 52) Bromoform 27.99 173 42152 4.77 ug/L 99 53) 1,1,2,2-Tetrachloroethane 28.26 83 105734 5.18 ug/L 98 55) 1,2,3-Trichloropropane 28.63 75 85376 5.18 ug/L 98 56) n-Propylbenzene 28.84 91 2049514 5.20 ug/L 100 57) Bromobenzene 29.07 77 450480 4.99 ug/L 100 58) 1,3,5-Trimethylbenzene 29.22 105 1347380 5.03 ug/L 100 59) 2-Chlorotoluene 29.37 91 1132428 5.15 ug/L 98 60) 4-Chlorotoluene 29.47 91 1078149 4.99 ug/L 97 61) tert-Butylbenzene 30.14 119 1192145 5.06 ug/L 99 62) 1,2,4-Trimethylbenzene 30.25 105 1374687 5.14 ug/L 99 63) sec-Butylbenzene 30.68 105 1909106 5.12 ug/L 100 64) p-Isopropyltoluene 31.01 119 1528377 4.77 ug/L 100 65) 1,3-Dichlorobenzene 31.37 146 591005 4.95 ug/L 99 66) 1,4-Dichlorobenzene 31.62 146 565950 4.93 ug/L 99 67) n-Butylbenzene 32.06 91 1469149 4.78 ug/L 100 68) 1,2-Dichlorobenzene 32.60 146 438448 4.90 ug/L 99 69) 1,2-Dibromo-3-chloropropan 34.65 157 14308 4.97 ug/L 98 70) Nitrobenzene , 34.92 77 36442 78.61 ug/L 96 71) 1,2,4-Trichlorobenzene 37.42 180 257750 4.78 ug/L 100 72) Hexachlorobutadiene 37.84 225 219377 5.18 ug/L 99 73) Naphthalene 38.41 128 291849 4.68 ug/L 100 74) 1,2,3-Trichlorobenzene 39.34 180 187070 4.81 ug/L 99

(#) = qualifier out of range (m) =; manual integration 0503R5.D W050302.M Fri May 03 17:03:21 2002 Page 2

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