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← Document results/DEP Box 63/ICP-MS Tuning File Jan 29 - Feb 14, 2002
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ICP-MS Daily Performance Check Report, Jan 29, 2002

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Laboratory report documenting daily instrument performance checks for ICP-MS analysis on January 29, 2002.

NYC-WTC_000076052–000076075

Folder label: “ICP-MS Tuning File Jan 29 - Feb 14, 2002

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NYC 9/11 Public Portal Document

Daily Performance Report Sample ID: DPC Sample Date/TIme: Thursday, January 31,200210:36:54 Sample Description: DAILY PERFORMANCE CHECK Method File: d:\elandata\MethocftDAILY PERF TO SAVE REPORT.mth Dataset File: d:\elandata\Datasettdaily performance\DPC.047 Tuning File: d:\elandata\Tuning\defaulttun Optimization File: d:\elandata\Optimize\defaultdac Dual Detector Mode: Pulse Acq. Dead Tlme(ns): 55 Current Dead Time (ns): 55

Summary Analyte Mass Meas. Intens. Mean Net Intens. Mean Net Intens. SD Net Intens. RSD Mg 24.0 70103.7 70103.747 670.720 1.0 Rh 102.9 291744.0 291743.967 3322.298 1.1 In 114.9 392051.0 392050.959 6747.591 1.7 Pb 208.0 244495.9 244495.917 6287.398 2.6 r> Ba 137.9 337276.7 337276.682 6643.941 2.0 L Ba++ 69.0 4661.2 0.014 0.000 2.0 r> Ce 139.9 418853.4 418853.435 7114.802 1.7 L CeO 155.9 11687.6 0.028 0.000 0.8 Bkgd 220.0 12.4 12.433 0.976 7.9

Current Optimization File Data Current Value Description 0.89 Nebulizer Gas Flow 6.25 Lens Voltage 1000.00 ICP RF Power -1887.50 Analog Stage Voltage 1500.00 Pulse Stage Voltage 70.00 Discriminator Threshold -6.00 AC Rod Offset 60.00 Service DAC 1 0.00 Quadrupole Rod Offeet

Current Autolens Data Analyte Mass Num of Pts DAC Value Maximum Intensity Be 9 21 5.8 7558.2 Al 27 21 6.0 179221.1 Sc 45 21 6.0 1010866.2 V 51 21 6.0 222947.9 Cr 52 21 6.3 202078.3 Mn 55 21 6.3 303423.5 Nl 58 21 6.0 128259.7 Co 59 21 6.3 223383.4 Cu 63 21 6.0 116913.1 Zn 64 21 6.3 63718.2 Cu 65 21 6.5 57939.6 Zn 66 21 6.3 38135.2 Zn 68 21 6.3 27276.1 Ge 74 21 6.5 265184.8 As 75 21 6.3 34129.3

Sample ID: DPC Report Date/Time: Thursday, January 31,200210:40:20 Pagel

NYC-WTC_000076056

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NYC-WTC_000076056Source: NYC Law Department, mirrored locally

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