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Water analysis report, Antimony, Nov 2001

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Lab report for NYC DEP water samples collected November 14, 2001, testing for antimony using ICPMS.

NYC-WTC_000070610–000070627

Folder label: “27872

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NYC 9/11 Public Portal Document

REPORT OF ANALYSIS Westchester County Department of Labs and Research 2 Dana Road Valhalla, New York

Agency: NYCDEP Bureau Water Sample NYC DEP 465 Columbus Ave. 19 WESTLAKE DRIVE Valhalla, NY 10595 VALHALLA, N.Y. Sample CROGH Attention: Steve Schindler ID of Source: Received EP Collection 11/14/2001 AT 9:05:00 Bottle c583,p909,876,877,q798,761 ,753 Submitted 11/14/2001 AT 1:25:00 Collected By: NEWMAN Sample Type: POT_DW Comment: PWS No.: Source Code: 000 Type Descriptor: Sample chilled on arrival? : yes Report

Sample No. AD27874 Method Test Description Results Units MDL Analyzed on Validator Butachlor <MDL ug/L 0.40 11/20/2001 DLV EPTC <MDL ug/L 1.0 11/20/2001 DLV Hexachlorobenzene <MDL ug/L 0.10 11/20/2001 DLV Hexachlorocyclopentadiene <MDL ug/L 0.10 11/20/2001 DLV Metolachlor <MDL ug/L 0.75 11/20/2001 DLV Metribuzin <MDL ug/L 0.15 11/20/2001 DLV Molinate <MDL ug/L 0.90 11/20/2001 DLV Simazine < MDL ug/L 0.40 11/20/2001 DLV Terbacil <MDL ug/L 2.0 11/20/2001 DLV The recoveries for 3 of the 18 compounds in the LCS Standard were outside of their acceptance ranges. The recoveries for 2 of the 18 compounds in the Spiked Sample were below their acceptance ranges. The breakdown for Endrin in the Breakdown Standard was 64%. This may be because the injection port is set at 280 degrees Celcius. An investigation will be performed to evaluate injection port parameters, GCMS Scan For Unknowns Other unknown compounds ug/L 1/2/2002 DLV A scan of the extract prepared for the 508 analysis, from 35-550 amu using a mass spectrometer, does not reveal the presence of non-target compounds.

Approved Pam Dilsizian QA Officer Date Approved: 2/4/2002

Environmental Laboratories emailed Original 2/4/2002

NYS ELAP # 10108 Page 6 of 6

NYC-WTC_000070627

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NYC-WTC_000070627Source: NYC Law Department, mirrored locally

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NYC-WTC_000070606 · Box DEP Box 61

Record documenting the chain of custody for samples submitted to the Westchester County Department of Labs and Research.

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