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Water analysis report, Beryllium and Calcium, Nov 2001

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Lab report for NYC DEP water samples collected November 13, 2001, testing for beryllium and calcium.

NYC-WTC_000070550–000070567

Folder label: “27773

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NYC 9/11 Public Portal Document

REPORT OF ANALYSIS Westchester County Department of Labs and Research 2 Dana Road Valhalla, New York

Agency: NYCDEP Bureau Water Sample NYC DEP 465 Columbus Ave. 19 WESTLAKE DRIVE Valhalla, NY 10595 VALHALLA, N.Y. Sample CROGH Attention: Steve Schindler ID of Source: Received EP Collection 11/13/2001 AT 9:08:00 Bottle c617,p846,832,834,q684,700,699 Submitted 11/13/2001 AT 2:31:00 Collected By: NEWMAN Sample Type: POT_DW Comment: PWS No.: Source Code: 000 Type Descriptor: Sample chilled on arrival? : yes Report

Sample No. AD27775 Method Test Description Results Units MDL Analyzed on Validator Butachlor <MDL ug/L 0.40 11/24/2001 DLV EPTC <MDL ug/L 1.0 11/24/2001 DLV Hexachlorobenzene <MDL ug/L 0.10 11/24/2001 DLV Hexachlorocyclopentadiene <MDL ug/L 0.10 11/24/2001 DLV Metolachlor < MDL ug/L 0.75 11/24/2001 DLV Metribuzin <MDL ug/L 0.15 11/24/2001 DLV Molinate <MDL ug/L 0.90 11/24/2001 DLV Simazine <MDL ug/L 0.40 11/24/2001 DLV Terbacil <MDL ug/L 2.0 11/24/2001 DLV The recoveries for 2 of the 18 compounds in the LCS Standard were below their acceptance ranges. The recoveries for 3 of the 18 compounds in the Spiked Sample were outside of their acceptance ranges. The breakdown for Endrin in the Breakdown Standard was 68%. The injection port is kept at 280 degrees Celcius which may be contributing to high Endrin Breakdown. An investigation into modifying injection port parameters will be made. GCMS Scan For Unknowns Other unknown compounds ug/L 1/2/2002 DLV A scan of the extract prepared for the 508 analysis, from 35-550 amu using a mass spectrometer, does not reveal the presence of non-target compounds.

Approved Pam Dilsizian QA Officer Date Approved: 2/4/2002

Environmental Laboratories emailed Original 2/4/2002

NYS ELAP #10108 Page 6 of 6

NYC-WTC_000070567

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NYC-WTC_000070567Source: NYC Law Department, mirrored locally

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NYC-WTC_000070546 · Box DEP Box 61

Record documenting the chain of custody for samples submitted to the Westchester County Department of Labs and Research.

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