GC/MS analysis report for sample AD25844, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25843.D vial: 10 Acq On : 20 Nov 2001 12:05 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.21 ug/1 218887 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Teritative ID MW MolPorm CAS# Qual 1 2-Pentanone,/4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 5-Hexen-2-Me 98 C6H10O 000109-49-9 9 3 Morpholin^ 4-methyl- 101 C5H11N0 000109-02-4 9 4 tert-But;^Hydrop e roxi de 90 C4H10O2 000075-91-2 9 Abundance y Scan 289 (7.694 min): 25843.D (-) mZz 42.95 100.00% 4t3

59 5000 101 83 7.40 7.60 7.80 8.00 ‘ I '' ■ ■I ‘ ‘ ' I ■' ' '1‘'I I ' ' ■ ■ I m7z 59.05 51.93% Tlfe-> 10 20 30 40 50 K) 70 80 90 100 110 Abundance #64275:2-Pentanone, 4-hydroxy-4-methyI- 4b

5000 59 m/z 100.95 23.62% 15 31 101 I I I • 1 I I ■ ' I ' I I ■ • ■ • 1 ■ ■ ■ I 1 ■ ■ ■ ■ I I Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1291:5-Hexen-2-one 4)3 T "7.^ 7.60 7.80 8.00 5000 m/z 58.05 19.71% 55 27 ‘ I ‘ ‘ ‘ ‘ I ‘ I 37 50 . I 69 ' I ‘ ‘ ‘ * I ‘ ‘ ‘ ’ I ’ * ’ ’ I ' ' ‘ ‘ I ’ ' ’ ‘ I ‘ ‘ 83 • I ‘ 98 ' ' I I ' ' ' ' 1 TiZz-> 10 20 30 40 50 60 70 80 90 100 110 .... Abundance #63448: Morpholine, 4-methyl- -r-T^ I I I I I I > --Y’. . 7 4|3 7.40 7.60 7.80 8.00 m/z 42.05 8.13% 5000

82 87 93 101 ,1 I I • ‘ ' I ‘ ‘ ‘ I ' ' ' 1'' ' ' ‘ I ' ' I ' 1 ' • ' ' I ' ' I ' ' ‘ ' I ' ‘ ' I' ‘ ‘ ' 1 10 a) 30 40 50 60 70 80 90 100 110 7.^' 7.60' 'w' 8.00

25843.D NP103001.M Wed Dec 05 15:36:18 2001 Page 1

NYC-WTC_000070194