GC/MS analysis report for sample AD25830, Dec 2001

NYC 9/11 Public Portal Document

Librairy Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV1901\25793.D Vial: 13 Acq On : 20 Nov 2001 3:01 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Hexanone, 4-hydroxy-5-methyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.42 0.42 ug/1 82971 1,4-Dichloroben2ene-d4 11.72 Hit# of 5 Tentsrt^ive ID MW MolForm, CAS# Qual 1 2-Hexanone, <hydroxy-5-methyl-3-pr 172 C10H20O2I 061141-74-0 78 2 2-Hexanoney 100 C6H12O 000591-78-6 72 3 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Methyl ^obutyl Ketone 100 C6H12O . 000108-10-1 64 Abundance / Scan 150 (6.419 min): 25793.D (-) m/z 42795 100.00% 43

58 5000

85 100 eno 6.20 6.40 6.60 6.80 ■ ^■^,,,,,1,I.. ...... . m/^ 58.05 54.52% 20 30 40 50 60 70 60 90 100 110 120 130 140 Abundance #15807:2-Hexanone. 4-hydroxy-5-methyl-3-propyl- 4j3

___ .'^.1 ... 5000 58 6.00 6.20 6.40 6.60 ROT 27 "mTz 5776^ 14.76% 72 I ‘ I •'' ‘ I ■ ' ■' 11 .1 ' i"' ■ ■ ■ I' ^9° 111''' I ■' ■ ■ I ■ 11 ■ 111111 ■ • I • I ■

il&-> 20 30 40 50 60 70 OT 90 100 110 120 130 140 (Abundance #63384:2-Hexanone 43

6.00 6.20 6.40 6.60 6.80 . 5000 58 m/z 41.05 11.43% 29 71 85 100 Ip , , , |i, ,1, , ... ..... iiZz-> 20 30 40 50 60 70 80 90 iro 110 120 130 140 Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyI- 43 6.66' 'e.^' 'e.^' 6,60 rot'

L. m/z 100.05 9.88% 58 5000 29

71 • 11 ■ ■ 1111 ■ 111 ‘ J. I 85 100 140 t10lSlM140 T * ’ ' * 1 ' * * ' 1* ‘ • I • • 30 40 50 60 70 ^090 opo 6.20 6,40 6.60 6.80

25793.D NP103001.M Wed Dec 05 15:21:08 2001 Page 1

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