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GCMS analysis results for sample AD25736, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25736 conducted on November 29, 2001, noting other unknown compounds.

NYC-WTC_000069907–000069917

Folder label: “GCMS Scan X 10/26/01 An 11/7/01

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Scanned page image, NYC-WTC_000069915
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25736.D Vial: 23 Acq On : 17 Nov 2001 12:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.41 0.43 ug/1 68536 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexa: ne 100 C6H12O 000591-78-6 87 2 2-Hexi .one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 3 Meth- Isobutyl Ketone 100 C6H12O 000108-10-1 52 4 2-Hl :anone, 4 -methyl -____________ 114 C7H14O 000105-42-0 50 Abundance / Scan 149 (6.411 min): 25736.D (-) m7z 42.95 100.00% 43

58

71 85 100 6.00 6.20 6.40 6.60 6.80 '' I..................... . m/z 58.05 62.73% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Sundance #1556: 2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 m/z 41.05 20.22% 27 1, , , , J,........ I ■n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:.2-Hexanone, 4-hydroxy-3-propyl- 4|3

58 6.00 6,20 a40 6,6q a8g 5000 29 m/ z 57.00 14.83%

100

Ti&-> ' I ' ' ' ' I ' ' ' ' I I ' ' ' I ' 20 30 40 50 J, ' ' I ' 60 70 71 I 85 I T-f-r-r-n-p-r-T- 80 I 90 100 110 I.. . ■, .. ,, ,1';^ 120 130 140 Abundance #63350: Methyl Isobutyl Ketone 413 6.00 6.20 6.40 6.60 6.80 m/z 100.00 12.27% 5000 58

85 100 27 67 I rr-r-TT-Tq-^n-T-T-q-TT-T-T^ Ma a ... ,|, 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

25736.D NP103001.M Thu Nov 29 09:21:25 2001 Page 1

NYC-WTC_000069915

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NYC-WTC_000069915Source: NYC Law Department, mirrored locally

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