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GCMS analysis results for sample AD25665, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25665 conducted on November 29, 2001, noting other unknown compounds.

NYC-WTC_000069852–000069862

Folder label: “GCMS Scan X 10/26/01 An 11/7/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV1601\25665.D Vial: 16 Acq On : 17 Nov 2001 5:40 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.418 147 150 157 rBV 21937 58686 1.14% 0.215% 2 7.685 284 288 306 rBV 120808 396367 7.71% 1.455% 3 11.715 721 727 749 rBV 1243835 3519920 68.45% 12.918% 4 15.314 1114 1119 1138 rBV 2061591 4646968 90.37% 17.054% 5 20.593 1688 1694 1714 rBV 2339581 5142409 100.00% 18.872% 6 25.017 2169 2176 2188 rBV2 2293521 4927919 95.83% 18.085% 7 25.155 2188 2191 2205 rVB2 17181 62402 1.21% 0.229% 8 33.050 3044 3051 3070 rBV2 1892351 4507446 87.65% 16.542% 9 37.154 3488 3498 3519 rBV2 1376386 3986756 77.53% 14.631%

Sum of corrected areas: 27248873 25665.D NP103001.M Wed Nov 28 14:20:30 2001

NYC-WTC_000069859

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NYC-WTC_000069859Source: NYC Law Department, mirrored locally

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