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GCMS analysis results for sample AD24949, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24949 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069117–000069127

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0601\24949.D Vial: 17 Acq On : 7 Nov 2001 4:22 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T, first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.440 148 152 163 rW 22055 58911 1.01% 0.195% 2 7.698 285 289 301 rBV 121223 317233 5.42% 1.050% 3 11.572 706 711 720 rBV 45116 104599 1.79% 0.346% 4 11.710 721 726 745 rW 1633127 3927520 67.09% 13.004% 5 15.318 1113 1119 1138 rBV 2524022 5399001 92.23% 17.876%

6 20.596 1687 1694 1714 rBV 2732681 5853816 100.00% 19.382% 7 25.021 2169 2176 2189 rBV2 2655797 5675877 96.96% 18.793% 8 33.063 3045 3052 3076 rBV2 2089272 4904471 83.78% 16.239% 9 37.167 3490 3499 3517 rBV 1376312 3961089 67.67% 13.115%

Sum of corrected areas: 30202517 24949.D NP103001.M Fri Nov 16 15:23:34 2001

NYC-WTC_000069123

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NYC-WTC_000069123Source: NYC Law Department, mirrored locally

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