GC/MS analysis results for sample AD25043, Nov 27 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0801\25043.D Vial: 4 Acq On : 8 Nov 2001 5:32 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

11.57 0.55 ug/1 142318 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenz^e-d4 150 C6C12D4 003855-82-1 50 2 Benzene-1,2,3,4/d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzaldehyde, ^-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 2-Methyl-6-n^roaniline_____________ 152 C7H8N2O2 000570-24-1 10 Abundance Scan 711 (11.569 min): 25043. D (-) ra/z 149.90 100.00% Iio

5000 115

52 78 40 1120 11.40 11.60 11.80 99 ■ • I >' ■ > 111 ■ 4^ m/z 151.90 67.29% t)A:-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 liiO

5000 115 78 11.20 11.40 11.60 11.80 52 m/z 114.90 42.13% 35 87 tX Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-, 5.6-dichloro- 1!i0 ............ 115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 21.75%

87

■nfe-> 30 35

40 50 60 70 I 80 90 A 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde. 2-hydroxy-3-methoxy- 1$2 11.20 11.40 11.60 11.80 Wz 52.00 16.65% 106 5000 53 81

'' ■ I ■'' ■ I' ■ 111' 92 122 I ' I ‘' I'''' I ...... "..pl??....... I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80

25043.D NP103001.M Mon Nov 19 15:07:08 2001 Page 2

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