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GCMS analysis results for sample AD25039, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25039 conducted on November 19, 2001, identifying unknown compounds.

NYC-WTC_000069234–000069244

Folder label: “GCMS Scan X 10/19/01 An 11/8/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV0801\25039.D Vial: 13 Acq On : 9 Nov 2001 2:19 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 9 3:08 2001 Quant Results File: NP103001.RES Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Pri Nov 02 16:41:16 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 152 960350 20.00 ug/1 -0.01 19) Naphthalene-d8 15.32 136 3747500 20.00 ug/1 -0.01 31) Acenaphthene-dlO 20.60 164 1889188 20.00 ug/1 -0.01 49) Phenanthrene-dlO 25.02 188 2815306 20.00 ug/1 -0.01 59) Chrysene-dl2 33.06 240 2085760 20.00 ug/1 0.00 68) Perylene-dl2 37.17 264 1652491 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.70 132 722 0.01 ug/1 0.46 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 11645 0.27 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.54% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.60 172 339 0.00 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.00% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 29.94 244 2205 0.02 ug/1 0.00 Spiked Amount 50.000 Recovery = 0.04% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration 25039.D NP103001.M Mon Nov 19 14:33:52 2001 Page 1

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NYC-WTC_000069236Source: NYC Law Department, mirrored locally

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