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GCMS analysis results for sample AD24699, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24699 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068866–000068879

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report •Data File : C:\HPCHEM\1\DATA\NOV0501\24699.D Vial: 18 Acq On : 6 Nov 2001 4:32 am Operator: 209 GALOS Sample : gc/ms unknown Inst J GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.305 134 137 143 rBV 25922 58276 1.26% 0.243% 2 6.415 145 149 159 rVV2 41322 128763 2.79% 0.537% 3 6.543 160 163 172 rW 24069 68598 1.49% 0.286% 4 6.663 172 176 193 r'VB 29053 88550 1.92% 0.370% 5 7.691 284 288 304 rBV 73504 244919 5.31% 1.022% 6 11.574 707 711 720 rBV 33740 83983 1.82% 0.350% 7 11.712 720 726 744 rBV 1223069 3173030 68.76% 13.240% 8 15.320 1113 1119 1138 rBV 1990312 4276674 92.68% 17.846% 9 20.599 1687 1694 1711 rBV 2122311 4614698 100.00% 19.256% 10 25.023 2169 2176 2188 rBV2 1975084 4388724 95.10% 18.313% 11 33.056 3044 3051 3075 rBV2 1606674 3755095 81.37% 15.669% 12 37.160 3490 3498 3522 rBV2 1116950 3083317 66.82% 12.866%

Sum of corrected areas: 23964627 24699.D NP103001.M Tue Nov 13 12:07:55 2001

NYC-WTC_000068872

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NYC-WTC_000068872Source: NYC Law Department, mirrored locally

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