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GC/MS analysis results, sample AD24482, November 2001

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AD24482 completed November 13, 2001, identifying other unknown compounds with violations referenced in comments.

NYC-WTC_000068748–000068762

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C;\HPCHEM\1\DATA\NOV0201\24482.D Vial: 21 Acq On 3 Nov 2001 10:28 am Operator: 209 GALOS Sample gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.304 133 137 143 rBV 31959 70728 1.74% 0.325% 2 6.414 145 149 160 rVV2 52761 154813 3.81% 0.712% 3 6.543 160 163 172 rW 28764 71517 1.76% 0.329% 4 6.662 172 176 185 rVB 33881 80723 1.99% 0.371% 5 7.690 284 288 304 rBV 63465 206431 5.08% 0.949% 6 11.573 705 711 721 rBV 30888 78819 1.94% 0.362% 7 11.711 721 726 746 rVB 1090698 2831759 69.69% 13.023% 8 15.319 1113 1119 1136 rBV 1822469 3871102 95.27% 17.803% 9 20.598 1687 1694 1713 rBV 1889830 4063313 100.00% 18.687% 10 25.023 2169 2176 2187 rBV 1716619 3835643 94.40% 17.640%

11 33.055 3043 3051 3074 rBV2 1535458 3536582 87.04% 16.265% 12 37.150 3489 3497 3513 rBV2 997773 2942570 72.42% 13.533%

Sum of corrected areas; 21744000 24482.D NP103001.M Fri Nov 09 14:54:22 2001

NYC-WTC_000068754

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NYC-WTC_000068754Source: NYC Law Department, mirrored locally

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