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GCMS analysis results for sample AD24290, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24290 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068158–000068170

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\OCT3101\24289.D Vial: 10 Acq On 1 Nov 2001 12:54 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.318 136 139 144 rBV 19223 40126 1.03% 0.195% 2 6.419 147 150 161 rW 30609 81320 2.08% 0.396% 3 6.666 174 177 184 rW 21249 43502 1.11% 0.212% 4 7.695 285 289 300 rBV 61801 166311 4.25% 0.810% 5 11.578 708 712 721 rBV 31236 72098 1.84% 0.351% 6 11.706 721 726 747 rBV 1082853 2806312 71.80% 13.672% 7 15.314 1114 1119 1134 rBV 1732269 3779869 96.71% 18.415% 8 20.593 1688 1694 1715 rBV 1839680 3908606 100.00% 19.042% 9 25.018 2169 2176 2187 rBV2 1751987 3668322 93.85% 17.871% 10 33.051 3044 3051 3069 rBV2 1419254 3206508 82.04% 15.622% 11 37.154 3489 3498 3509 rBV 987288 2753193 70.44% 13.413%

Sum of corrected areas: 20526167 24289.D NP103001.M Fri Nov 02 12:01:29 2001

NYC-WTC_000068164

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NYC-WTC_000068164Source: NYC Law Department, mirrored locally

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