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GCMS analysis results for sample AD24216, Nov 6 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24216 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000067990–000068002

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV0101\24215.D Vial: 2 Acq On 1 Nov 2001 4:00 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.419 146 150 160 rVV2 34044 98580 1.69% 0.320% 2 7.685 284 288 303 rBV 91571 259950 4.46% 0.844% 3 11.569 705 711 721 rBV 47060 115158 1.98% 0.374% 4 11.706 721 726 743 rW 1611134 4065890 69.76% 13.197% 5 15.323 1113 1120 1137 rBV 2492316 5598226 96.05% 18.170% 6 20.602 1688 1695 1712 rBV 2688236 5828523 100.00% 18.918% 7 25.027 2170 2177 2190 rBV 2520388 5517944 94.67% 17.910% 8 33.060 3044 3052 3071 rBV2 2099681 5016635 86.07% 16.283% 9 37.163 3488 3499 3517 rBV2 1497450 4308614 73.92% 13.985%

Sum of corrected areas: 30809520 24215.D NP103001.M Tue Nov 06 11:44:32 2001

NYC-WTC_000067996

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NYC-WTC_000067996Source: NYC Law Department, mirrored locally

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