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GCMS analysis results for sample AD24641, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24641 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068672–000068683

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068678
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File C:\HPCHEM\1\DATA\NOV0 501\24641.D Vial: 11 Acq On 5 Nov 2001 9:44 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering; 5 Sampling ; 1 Min Area; 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal ; TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.428^ 148 151 162 rW 40633 100535 1.82% 0.348% 2 7.694^ 286 289 300 rBV 59608 160551 2.90% 0.555% 3 11.578^ 707 712 721 rBV 41009 105420 1.91% 0.365% 4 11.706^ 721 726 749 rW 1477102 3752305 67.89% 12.982% 5 15.314>^ 1113 1119 1138 rBV 2287048 5098736 92.25% 17.640%

6 20.593'' 1688 1694 1718 rBV 2494417 5526797 100.00% 19.121% 7 25.018^ 2170 2176 2188 rBV2 2378591 5377528 97.30% 18.604% 8 33.060^ 3045 3052 3065 rBV2 2017159 4778221 86.46% 16.531% 9 37.163^ 3490 3499 3515 rBV2 1371028 4004623 72.46% 13.855%

Sum of corrected areas: 28904716 24641.D NP103001.M Fri Nov 09 12:16:06 2001

NYC-WTC_000068678

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NYC-WTC_000068678Source: NYC Law Department, mirrored locally

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