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GCMS calibration table for TCLP analysis, Nov 2001

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Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.

NYC-WTC_000068559–000068571

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV0501\LB.D Vial; 2 Acq On : 5 Nov 2001 12:14 pm Operator; 209 GALOS Sample : 10/16 lab blk Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: RTEINT.P Quant Time; Nov 5 13:04 2001 Quant Results File; NP103001.RES Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Last Update ; Fri Nov 02 16:41:16 2001 Response via ; Initial Calibration DataAcq Meth : NP103001

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol . 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 20.94 165 210 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.03 178 608 N.D. 56) Anthracene 25.03 178 608 N.D. 57) Di-n-butylphthalate 27.03 149 2886 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 29.21 184 5058 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.07 228 3515 N.D. 66) Bis(2-ethylhexyl)phthalate 33.33 149 1703 N.D. 67) Chrysene 33.07 228 3515 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 7 0) Benzo(b)fluoranthene 0.00 252 0 N.D. (#) = qualifier out of range (m) = manual integration LB.D NP103001.M Wed Nov 07 12:45:39 2001 Page 2

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