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GCMS analysis results for sample AD24480, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24480 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068529–000068543

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0201\24480.D Vial: 18 Acq On 3 Nov 2001 7:34 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Thtegrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.66 0.64 ug/1 88216 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexa: 1 102 C6H14O 000626-93-7 78 2 2-Hexi .ol, (R) - 102 C6H14O 026549-24-6 78 3 2-» :anol, (S)- 102 C6H14O 052019-78-0 78 4 2- ;ntanol, 4-methyl- 102 C6H14O 000108-11-2 64 4bundande Scan 176 (6.661 min): 24480.D (-) m/z 44.95 100.00% 4|5

250

69 6.40 6.60 6.80 7.00 50 55 I 87 100 " I ‘' I''" I Wz 69700 13.42% Ti/z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

4 #63584: 2-Hexanol (I 5000 __6;4g_6;60__a80__7W__ 69 m/z 40795 12.47% . ”4.,... ,„ii 56 ^++- 11I" 1111'1111.11111111111.1 I I" " I" " I" ‘' I . Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1794: 2-Hexanol, (R)- 45

6,40 6.60 6.80 7.00 5000 m/z 42.95 10.96%

69 87 ”.. .... ■n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1769: 2-Hexanol. (S)- ______ 45 __6;4g_6J60_a80_^W__ m/z 44700 10.72% 5000

re y 87 TT-tl I > ■ ■ ■ I I ■ I I I I I I > I I I I I I I . . I I I I . I I . . I , | l I I . I ■ ■ ■ ■ I I I I I J I . . . I I I . I I n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

24480.D NP103001.M Tue Nov 13 10:12:53 2001 Page 4

NYC-WTC_000068540

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NYC-WTC_000068540Source: NYC Law Department, mirrored locally

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