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GCMS analysis results for sample AD24293, Nov 7 2001

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Laboratory report documenting GCMS analysis of sample AD24293 conducted on November 7, 2001, noting unknown compounds.

NYC-WTC_000068198–000068212

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report , Data File : C:\HPCHEM\1\DATA\OCT3101\24292.D Vial: 11 Acq On : 1 Nov 2001 1:52 am Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.313 134 138 144 rBV 21741 48110 1.23% 0.231% 2 6.414 146 149 160 rW 36351 106331 2.71% 0.511% 3 6.543 160 163 171 rW 21452 58362 1.49% 0.281% 4 6.662 172 176 192 rVB 26111 74127 1.89% 0.357% 5 7.690 284 288 305 rBV 60360 201031 5.13% 0.967%

6 11.574 706 711 721 rBV 29224 71677 1.83% 0.345% 7 11.711 721 726 748 rVB 1060366 2773595 70.80% 13.341% 8 15.319 1113 1119 1138 rBV 1831524 3786258 96.65% 18.212% 9 20.598 1687 1694 1712 rBV 1869065 3917618 100.00% 18.844% 10 25.023 2169 2176 2187 rBV 1651653 3602043 91.94% 17.326%

11 33.056 3043 3051 3071 rBV2 1406029 3301864 84.28% 15.882% 12 37.150 3489 3497 3509 rBV2 988030 2849071 72.72% 13.704%

Sum of corrected areas: 20790087 24292.D NP103001.M Fri Nov 02 12:04:36 2001

NYC-WTC_000068204

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NYC-WTC_000068204Source: NYC Law Department, mirrored locally

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