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GCMS analysis results for sample AD24288, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24288 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068131–000068144

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : Cs\HPCHEM\1\DATA\OCT3101\24287.D Vial: 8 Acq On : 31 Oct 2001 10:57 pra Operator: 209 GALOS Saraple : gc/ras unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Pararas: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Sraoothing : OFF Filtering: 5 Sarapling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first raax last PK peak peak peak % of # rain scan scan scan TY height area % raax. total 1 6.319 135 139 145 rBV 20497 43416 1.14% 0.215% 2 6.420 146 150 161 rVV2 35773 98339 2.58% 0.488% 3 6.558 161 165 173 rW 18535 49857 1.31% 0.247% 4 6.668 173 177 192 rVB2 24363 61720 1.62% 0.306% 5 7.696 285 289 304 rBV 55490 165138 4.33% 0.819% 6 11.570 707 711 721 rBV 27862 71089 1.86% 0.353% 7 11.708 721 726 747 rW 1035964 2721892 71.40% 13.505% 8 15.316 1113 1119 1137 rBV 1699767 3669181 96.24% 18.205% 9 20.594 1688 1694 1709 rBV 1830371 3812372 100.00% 18.916% 10 25.019 2169 2176 2188 rBV2 1672686 3587499 94.10% 17.800% 11 33.052 3044 3051 3073 rBV2 1357671 3159085 82.86% 15.674% 12 37.156 3489 3498 3514 rBV2 953816 2714749 71.21% 13.470%

Sura of corrected areas: 20154337 24287.D NP103001.M Fri Nov 02 11:59:41 2001

NYC-WTC_000068137

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NYC-WTC_000068137Source: NYC Law Department, mirrored locally

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