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GCMS analysis results for sample AD24238, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24238 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068101–000068116

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24237.D Vial: 4 Acq On : 31 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.33 0.44 ug/1 60676 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForra CAS# Qual 1 3-Hexar^ne 100 C6H12O 000589-38-8 64 2 Heptane, 3,3-dimethyl- 128 C9H20 004032-86-4 47 3 Hexane, 3,3,4-trimethyl- 128 C9H20 016747-31-2 47 4 3 - P^tanone, 2 -methyl - 100 C6H12O 000565-69-5 47 Scan 140 (6.326 min): 24237.D (-) mTz 43.00 100.00% 43 57

71 5000 100

.. ................... . 6.00 6.20 6.40 6.60 4-r'- m/z 57.00 90.07% Ti/z-> 20 30 40 50 60 70 80 90 100 1101M (1 Abundance #63357; 3-Hexanone 40 57 29 5000 71 '6.00 ' 6.^ ' ' 6,« 6.60 100 m/z 71.0.0 62.52% . ............ ............ ■ I ' ■ ■ ' I ' nfe-> 20 30 40 50 60 70 80 90 100 110 Abundance #5139; Heptane, 3,3-dimethyl- 43 5)7 71 6.00 6.20 6.40 6.60 5000 m/z 100.05 45.90% 27 39 I 35 , TiZz-> 20' " 30' ‘ ' '40 50 60 70 80 90 100 110 120 Abundance #5135: Hexane. 3,3.4-trimethyl- 43 57 71 6.00 6.20 6.40 6.60 ■m/z 41.05 27.31% 5000

27 39 ■ I,............................ 1............ 113 +-n nfe-> 20 30 40 60 70 80 90 100 110 120 6.00 6.20 6.40 6.60

24237.D NP103001.M Fri Nov 02 11:57:34 2001 Page 1

NYC-WTC_000068109

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NYC-WTC_000068109Source: NYC Law Department, mirrored locally

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