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GCMS analysis results for sample AD24238, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24238 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068101–000068116

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report *• Data File : C:\HPCHEM\1\DATA\OCT3101\24237.D Vial: 4 Acq On : 31 Oct 2001 7:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.326 136 140 147 rBV 29646 60676 1.51% 0.290% 2 6.427 147 151 160 rVV2 45883 116537 2.90% 0.558% 3 6.555 162 165 174 rW 25430 63394 1.58% 0.303% 4 6.675 174 178 190 rVB 34283 76090 1.90% 0.364% 5 7.694 285 289 301 rBV 129407 332297 8.28% 1.590% 6 11.577 707 712 721 rBV 30294 74341 1.85% 0.356% 7 11.715 721 727 746 rBV 1118545 2772609 69.06% 13.268% 8 15.323 1114 1120 1136 rBV 1743541 3842724 95.72% 18.389% 9 20.601 1688 1695 1707 rBV 1832635 4014524 100.00% 19.212% 10 25.017 2170 2176 2188 rBV2 1771674 3827955 95.35% 18 .319% 11 33.059 3045 3052 3064 rBV2 1288684 3141527 78.25% 15.034% 12 37.153 3489 3498 3517 rBV 942526 2573726 64.11% 12.317%

Sum of corrected areas: 20896400 24237.D NP103001.M Fri Nov 02 11:57:27 2001

NYC-WTC_000068107

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NYC-WTC_000068107Source: NYC Law Department, mirrored locally

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