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GCMS analysis results for sample AD23996, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD23996 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067767–000067781

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : Cs\HPCHEM\l\DATA\OCT2501\23996.D Vial: 4 Acq On : 25 Oct 2001 3:37 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.35 0.54 ug/1 101986 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone/ 100 C6H12O 000589-38-8 91 2 3-Pentaiiprie, 2-methyl- 100 C6H12O 000565-69-5 47 3 Pentane", 3-bromo- 150 C5HllBr 001809-10-5 43 4 Pen^he, 2,3,4-trimethyl-_________ 114 C8H18 000565-75-3 40 Abundance"' Scan 143 (6.354 min): 23996.D (-) m/z 43.05 100.00% 4|3 57

71 (1 5000 100

600 6.20 6.40 6.60 ' I" ■ ■ I"' itI 4- m/z 577^7 90775% Tife-> . 20 30 40 50 60 70 80 M1M1101M 130 140 1M Abundance #63358; 3-Hexanone 43 57

5000 71 600 6.20 6.40 6.60 100 m/z 71760 63.55% ■ I •»*n ii&-> 20 30 40 60 70 80 90 100 110 120 130 140 150 Abundance #63397:3-Pentanone, 2-inethyl- 5k 43 6,00 " 6.^ 6.^ " 6.60 5000 29 m/z 100.05 32.05% 71 100 I jL. 1 85 I JI... I.... J, nZz-> 20 30 40 50 60 70 80 90 ioo’ iio '146'1^ Abundance #66684: Pentane. 3-bromo- 43 71 6.00 6.20 6.40 6.60 m/z 41.05 26.56% 5000

27 55 4- I 123 -p-TT I ' ' ‘' I 150 mfe-> 20 30 40 03' 70 80 90 100 110 120 130 140 150 6.00 6.20 6.40 6.60

23996.D NP101901.M Fri Oct 26 10:09:38 2001 Page 1

NYC-WTC_000067775

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NYC-WTC_000067775Source: NYC Law Department, mirrored locally

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