GCMS analysis report, sample AD22558, October 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\22558.D Vial: 3 Acq On : 17 Oct 2001 3:08 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.37 0.53 ug/1 50536 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexan( e 100 C6H12O 000589-38-8 91 2 2,4-Pe: anedione 100 C5H8O2 000123-54-6 38 3 Hepta: , 3,3-dimethy1- 128 C9H20 004032-86-4 36 4 3-Pe: anone, 2-methyl- 100 C6H12O 000565-69-5 33 Abundance . Scan 145 (6.374 min): 22558.D (-) m/z 43.00 100.00% 43 57

71 5000 100 ■

6.Z) 6.40 6.M 6.M I... m/z 57.00 88.02% ttZz-> 20253035404550556065 70 75 80859095 100105110115120 Abundance #63358:3-Hexanone 43 57

71 5000 6.00 6.20 6.40 6.60 6.80 100 m/^ 71.00 59.73% 85 +^T nfe-> 20253035404550556065 70 75 80859095 100105110115120 Abundance #63324:2,4-Pentanedione 43

6.00 6.20 6.40 6.60 6.80 5000 85 m/z 100.05 33.15% 100

58 72 20253035404550556065 70 75 80859095 100105110115120 Abundance #5139: Heptane, 3,3-dimethyl- \J ■ I • ■ ■ ■ I • ■ ■ ■ I • ■ ' I ■ ' ' ' I ' 43 5|7 6.00 6.20 6.40 6.60 6.80 71 “m/z 41.05 24.69% 5000

27 I I n&-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 6.00 6.20 6,40 6.60 6.80

22558.D NP101901.M Tue Oct 23 15:08:14 2001 Page 1

NYC-WTC_000067414