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Duplicate spike results, sample AD22652, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report for a spiked sample AD22652 used to verify recovery rates of pesticides and organic compounds in late September 2001.

NYC-WTC_000063513–000063517

Folder label: “525 9/25/01 Extr 9/30 Analysis

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z z -< o o co § '2 o o Integration Report Quanfile: 22652MSD Quan Entries: 28 ■a c CT o' o O) Ca3 Comment: BOHLK; METHOD 525; INST 204; 09/30/01; SAMPLE 22652 MSD ■D o O1 Sorted via: Entry Number t 03 O) O o No Name of Compound R Time Scan# Mode Peak Ar0a PR Height o c 3 CD 3 chrysene d-12(IS> 22:58 1378 Auto 1,462,330 610,901 2- 4 p-terphenyl d-14(IS) 21:02 1262 Auto 2,631,411 1,988,405 5 acenaphthene d-10 C SURR 12:33 753 Auto 1,378,096 925,467 6 phenanthrene d-10(SURR 17:17 1037 Auto 2,130,387 1,016,604 7 chrysene d-12 (SURR) 22:58 1378 Auto 1,462,330 610,901 8 1,3-d imethy1-2-n itrobe 8:12 492 Auto 814,254 361,723 9 tr i pheny1 phosphate (S 22:20 1340 Auto 1,188,486 496,251 10 perylene d-12 (SURR) 27:32 1652 Auto 814,625 154,170 11 hexachlorocyclopentad i 10:23 623 Auto 428,622 209,963 12 hexachlorobenzene 15:44 944 Auto 641,090 268,895 13 simazine 16:31 991 Auto 582,408 169,759 14 atrazine 16:42 1002 Auto 527,793 209,642 15 alachlor 18:38 1118 Auto 814,273 571,794 16 bis(2-ethylhexyl)adipa 22:12 1332 Auto 1,371,699 559,545 17 bis(2-ethylhexy1Jphtha 23:15 1395 Auto 2,345,949 855,271 18 benzo(a)pyrene 27:17 1637 Auto 1,046,347 210,472 19 eptc 10:48 648 Auto 2,674,243 1,458,867 20 2,6-d in itrotoluene 12:10 730 Auto 540,333 339,150 21 2,4-d in itrotoluene 13:09 789 Auto 735,970 434,595 22 mol inate 13:18 798 Auto 1,486,169 1,047,045 23 terbac i1 17:41 1061 Auto 801,443 246,924 24 acetochlor 18:27 1107 Auto 597,659 316,494 25 metribuzin 18:29 1109 Auto 830,345 502,112 26 metolachlor 19:22 1162 Auto 2,435,5^ 1,434,065 27 butachlor 20:34 1234 Auto 863,650 592,857 28 4,4^-dde 20:58 1258 Auto 862,312 549,742

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NYC-WTC_000063516Source: NYC Law Department, mirrored locally

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