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Spiked sample results, sample AD22652, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report for reference standards used to validate the analysis of sample AD22652 conducted in late September 2001.

NYC-WTC_000063508–000063512

Folder label: “525 9/25/01 Extr 9/30 Analysis

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§ s o o o Integration Report Quanfile: 22652MS Quan Entries: 28 ■D c CT o' CD Comment: BOHLK; METHOD 525; INST 204; 09/30/01; SAMPLE 22652 MS "0 o Ca5 tn Sorted uia: Entry Number t 03

O o No Name of Compound R Time Scan# Mode Peak Ar^a PR Height o c 3 CD 3 chrysene d-12(IS) 22:58 1378 Auto 1,246,750 547,762 3

4 p-terphenyl d-14(IS) 21:02 1262 Auto 2,303,821 1,298,719 5 acenaphthene d-10CSllRR 12:33 753 Auto 1,501,056 892,056 6 phenanthrene d-10(SURR 17:17 1037 Auto 2,244,349 1,145,454 7 chrysene d-12 (SURR) 22:58 1378 Auto 1,246,750 547,762 8 1,3-d imethy1-2-n itrobe 8:13 493 Auto 868,499 465,725 9 triphenyl phosphate CS 22:20 1340 Auto 1,144,060 481,991 10 perylene d-12 (SURR) 27:32 1652 Auto 623,089 115,462 11 hexachlorocyclopentadi 10:24 624 Auto 458,567 293,749 12 hexachlorobenzene 15:44 944 Auto 691,221 297,819 13 simazine 16:31 991 Auto 580,473 175,328 14 atrazine 16:42 1002 Auto 524,617 197,560 15 alachlor 18:38 1118 Auto 838,550 374,542 16 bis(2-ethyIhexy1)ad ipa 22:12 1332 Auto 1,383,086 637,149 17 b is(2-ethyIhexy1)phtha 23:15 1395 Auto 2,243,264 788,971 18 benzo(a)pyrene 27:18 1638 Auto 772,258 138,577 19 eptc 10:48 648 Auto 2,895,410 2,001,785 20 2,6-d in itrotoluene 12:10 730 Auto 631,232 324,525 21 2,4-d in itrotoluene 13:09 789 Auto 716,882 347,468 22 molinate 13:18 798 Auto 1,553,461 1,042,410 23 terbac i1 17:41 1061 Auto 836,623 292,840 24 acetochlor 18:28 1108 Auto 593,143 290,159 25 metribuzin 18:29 1109 Auto 881,756 384,354 26 metolachlor 19:22 1162 Auto 2,582,540 1,538,235 27 butachlor 20:35 1235 Auto 738,072 333,101 28 4,4'-dde 20:58 1258 Auto 944,475 743,910

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NYC-WTC_000063511Source: NYC Law Department, mirrored locally

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